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Determination of nitrogen in nitrated petroleum products

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Chemistry and Technology of Fuels and Oils Aims and scope

Summary

  1. 1.

    The Kjeldahl method may be used to determine the total nitrogen content of nitrated petroleum products.

  2. 2.

    Data cited for the nitrogen content of various nitrated petroleum products indicate that the Kjeldahl method is sufficiently accurate to determine relative changes in the nitrogen content of nitration products in relation to the chemical composition of the raw material, nitration reaction conditions, and other factors.

  3. 3.

    It is shown that hydrocarbon nitration occurs when mineral oils or other high-boiling petroleum products interact with medium-concentration nitric acid.

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Literature cited

  1. A. L. Dol'berg and A. S. Grishaeva, Khim. i Tekhnol. Topliv i Masel, No. 1 (1964).

  2. R. P. Lastovskii and Yu. I. Vainshtein, Industrial Analysis and Production of Intermediates and Dyes [in Russian], Goskhimizdat (1958).

  3. J. Rosin, Reagent Chemicals and Standards (1955), p. 501.

  4. Guben-Veil, Methods of Organic Chemistry [in Russian], Vol. II, Goskhimizdat (1963), p. 633.

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  5. A. P. Terent'ev and B. M. Luskina, Organic Analysis [in Russian], Izd. AN SSSR (1963).

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Author information

Authors and Affiliations

  1. Moscow “Neftegaz” Plant, USSR

    A. L. Dol'berg

Authors
  1. A. L. Dol'berg
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Additional information

Laboratory workers S. S. Frolova and E. I. Koré took part in this work.

Translated from Khimiya i Tekhnologiya Topliv i Masel, No. 7, pp. 47–50, July, 1966.

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Dol'berg, A.L. Determination of nitrogen in nitrated petroleum products. Chem Technol Fuels Oils 2, 497–500 (1966). https://doi.org/10.1007/BF00725980

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  • DOI: https://doi.org/10.1007/BF00725980

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