Conclusions
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1.
A method has been worked out for preparing return raw material for the oxidation process, consisting of treating the unsaponifiables with a water solution of the low-molecular organic acids which is obtained in the form of an aqueous condensate in the manufacture of synthetic fatty acids, with separation of the salt solution in an electrical field.
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2.
The use of a dc electrical field reduces the settling time for unsaponifiables 10- to 12-fold and improves the completeness of separation of sodium salts from unsaponifiables.
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3.
The use of return raw material which has been treated with acid water makes it possible to stabilize the oxidation process, reduce the oxidation time by a minimum of 30%, and reduce the air consumption by at least a factor of 1.4.
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Literature cited
D. F. Varfolomeev, A. A. Kashin, and R. N. Khairullin, Neftepererabotka i Neftekhimiya, No. 8 (1969).
P. G. Igonin, V. P. Konoplev, V. V. Svitkin, and V. S. Dorodnova, Author's Certificate No. 263800; Byull. Izobret., No. 8 (1970).
V. P. Konoplev and Ya. I. Pinkovskii, Khim. i Tekhnol. Topliv i Masel, No. 4 (1969).
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Translated from Khimiya i Tekhnologiya Topliv i Masel, No. 9, pp. 21–23, September, 1972.
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Igonin, P.G., Svitkin, V.V., Dorodnova, V.S. et al. Preparation of return raw material for paraffin oxidation. Chem Technol Fuels Oils 8, 668–671 (1972). https://doi.org/10.1007/BF00717967
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DOI: https://doi.org/10.1007/BF00717967