Conclusions
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1.
In the preparation of lithium lubricants based on Ester 2 and L-ZP, a change in the heating rate from 1 to 10°C/min, within the limits from room temperature up to 200°C, does not lead to a change in the quality of the lubricant obtained. The heating time up to complete melting of the soap should be at a minimum.
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2.
For lubricants based on Ester 2, the most effective means is cooling in a layer with a thickness of not more than 3 mm, at a rate of 30°C/min.
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3.
Lubricants based on Ester L-ZP may be obtained with cooling both in a thin (3 mm) and in a thick (up to 20 mm) layer. The cooling rate may vary within the limits from 30 to 3.5°C/min without changing the quality of the lubricant obtained.
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Translated from Khimiya i Tekhnologiya Topliv i Masel, No. 7, pp. 27–29, July, 1971.
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Bukhovtseva, A.P., Krakhmalev, S.I. & Klimov, K.I. Special features of the preparation of lithium lubricants based on complex esters. Chem Technol Fuels Oils 7, 509–512 (1971). https://doi.org/10.1007/BF00716863
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DOI: https://doi.org/10.1007/BF00716863