Summary
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1.
The DL and DS grades of diesel oil, with boiling ranges 180–350°C, cannot be obtained from Mangyshlak petroleum owing to the high setting point. The setting point is conveniently reduced to the standard value by deparaffination of the end 250–350°C fraction and mixing with the 180–250°C undeparaffinized initial fraction.
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2.
The 250–350° fraction can be deparaffinized in a solution of dichloroethane. By cooling to −20°C we obtain a diesel fuel component with setting point −14°C.
Diesel fuel of DS grade with boiling range 180–350°C, obtained by mixing the head fraction with the deparaffinized end fraction, has a setting point of −18°C.
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3.
By a single repulping in dichloroethane of the slack wax obtained by deparaffinization of the 250–350° fraction, followed by filtration at −20°C, we obtain paraffin with setting point 28°C and 0.2% aromatic compounds, without finishing.
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Literature cited
M. G. Mitrofanov, O. A. Artem'eva, and A. G. Martynenko, Proc. of the 2nd Scientific and Technical Conference of GrozNII [in Russian], Chechingizdat (1957).
N. F. Bogdanov, S. I. Stepuro, L. P. Rozova, A. N. Pereverzev, and L. V. Pavlov, Tr. GrozNII, No. 20, Izd. Khimiya (1966).
N. F. Bogdanov and A. N. Pereverzev, Deparaffinization of Crude Oils [in Russian], Gostoptekhizdat (1961).
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Translated from Khimiya i Tekhnologiya Topliv i Masel, No. 4, pp. 19–21, April, 1968.
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Mitrofanov, M.G., Berezyuk, F.A., Karaibog, E.V. et al. Production of diesel fuel from Mangyshlak petroleum. Chem Technol Fuels Oils 4, 255–257 (1968). https://doi.org/10.1007/BF00715665
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DOI: https://doi.org/10.1007/BF00715665