Conclusions
-
1.
Five O,O-dialkyl-S-(N-β-aminoethyl)-carbamoylmethyl dithiophosphates and five methylenebis-(O,O-dialkyl-S-carbamoylmethyl dithiophosphates) were synthesized. The synthesized compounds were isolated in pure form by thin layer chromatography.
-
2.
It was found that the prepared compounds markedly increase the thermooxidative stability of lubricating oils.
Similar content being viewed by others
Literature cited
J. P. McDermott, U. S. Pattent 2,610,182 (1952); 2,766,207 (1956).
D. W. Dinsmore and A. H. Smith, U.S. Patent 3,002,014 (1961); 3,103,492 (1963).
S. E. Krein et al. (editors), Oil and Fuel Additives [in Russian], Gostoptekhizdat (1961).
A. F. Millikan, U.S. Patent 2,894,951 (1959).
J. J. McBride, U.S. Patent 2,766,208 (1956).
W. Lowe, U.S. Patent 3,184,412 (1965); 3,185,643 (1965).
J. O. Clayton, U.S. Patent 3,185,645 (1965).
E. O. Hook and P. H. Moss, U.S. Patent 2,586,656 (1952).
Y. R. Morris and N. I. Fichkill, U.S. Patent 2,736,707 (1956).
E. T. Wierber, U.S. Patent 3,284,548 (1966).
W. M. Le Suer, French Patent 1,367,789 (1964); 1,351,395 (1964); U.S. Patent 3,197,405 (1965).
B. Buchner and G. Curtis, U.S. Patent 3,286,001 (1966).
J. P. McDermott, U.S. Patent 2,743,235 (1956).
V. I. Isagulyants and G. I. Volotova, Zh. Prikl. Khim.,43, No. 4 (1970).
T. Ambrus, L. Tincu, C. Marculescu, and N. Barbulescu, Rev. Chim.,15, 386 (1964).
S. R. Palit et al., Nonaqueous Titration [Russian translation], Goskhimizdat (1958).
A. A. Akhrem and A. I. Kuznetsova, Thin Layer Chromatography [in Russian], Izd. Nauka (1965).
L. Bellamy, Infrared Spectra of Complex Molecules [Russian translation], Izd. Mir (1962).
Author information
Authors and Affiliations
Additional information
Translated from Khimiya i Tekhnologiya Topliv i Masel, No. 8, pp. 27–30, August, 1972.
Rights and permissions
About this article
Cite this article
Isagulyants, V.I., Bolotova, G.I., Parfenova, V.A. et al. Synthesis and study of ash-free lubricating oil additives. Chem Technol Fuels Oils 8, 594–596 (1972). https://doi.org/10.1007/BF00713908
Issue Date:
DOI: https://doi.org/10.1007/BF00713908