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Convenient method of synthesis of Cp2TaH3

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Abstract

Modified method for preparation of Cp2TaH3 by reaction between TaCl5, CpNa, and LiAlH4 in dimethoxyethane is described: The yield of Cp2TaH3 is 25 %.

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References

  1. T. M. Zvukova, A. I. Sizov, Yu. I. Gun'ko, B. M. Bulychev, and G. L. Soloveychik,Metalloorgan. Khim., 1988,1, 1179 [J. Organomet. Chem. USSR, 1988,1 (Engl. Transl.)].

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Authors and Affiliations

  1. Department of Chemistry, M. V. Lomonosov Moscow State University, Vorob'evy Gory, 119899, Moscow, Russian Federation

    T. M. Zvukova & A. I. Sizov

Authors
  1. T. M. Zvukova
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  2. A. I. Sizov
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Additional information

Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 10, pp. 2050–2051, October, 1995.

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Zvukova, T.M., Sizov, A.I. Convenient method of synthesis of Cp2TaH3 . Russ Chem Bull 44, 1970 (1995). https://doi.org/10.1007/BF00707241

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  • DOI: https://doi.org/10.1007/BF00707241

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