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Preparative synthesis of disilane from hexaethoxydisilane and diisobutylaluminum hydride

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Abstract

A preparative method for the synthesis of Si2H6 from Si2(OEt)6 and (i-Bu)2AlH is developed.

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References

  1. E. P. Belov, E. N. Lebedev, Yu. P. Grigorash, A. I. Gorbunov, and I. N. Litvinenko,Monosilan v Tekhnologii Poluprovodnikovykh Materialov, [Monosilane in the Technology of Semiconducting Materials], GNIIKhTEOS NIITEKhIM, Moscow, 1989, p. 34 (in Russian).

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  2. A. I. Kuznetsov,Zhurn. Prikl. Khimii, 1978,51, 1833, [J. Appl. Chem. 1978 (Engl. Transl)].

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  3. H. Azuhiko, V. Kadzo, and T. Masao, Patent 62-30612 Japan.

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Authors and Affiliations

  1. Research Institute of Chemistry and Technology of Organoelement Compounds, 38 sh. Entuziastov, 111123, Moscow, Russian Federation

    N. N. Korneev, G. I. Belik, E. P. Belov, N. N. Govorov, N. R. Karimova, E. N. Lebedev & I. A. Yushkevich

Authors
  1. N. N. Korneev
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  2. G. I. Belik
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  3. E. P. Belov
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  4. N. N. Govorov
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  5. N. R. Karimova
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  6. E. N. Lebedev
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  7. I. A. Yushkevich
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Additional information

Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 4, pp. 795–796, April, 1993.

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Korneev, N.N., Belik, G.I., Belov, E.P. et al. Preparative synthesis of disilane from hexaethoxydisilane and diisobutylaluminum hydride. Russ Chem Bull 42, 764–765 (1993). https://doi.org/10.1007/BF00704023

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  • DOI: https://doi.org/10.1007/BF00704023

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