Synthesis of methyl ethers of methyl (methyl α-D-glucopyranosid)uronate
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Methyl (methyl α-D-glucopyranosid)uronate (I) has been obtained by the catalytic oxidation of methyl α-D-glucopyranoside with oxygen in the presence of platinum on carbon with a yield of 31%. The partial methylation of (I) followed by preparative liquid column chromatography on silica gel has provided a convenient method of obtaining all the methyl ethers of (I) in the individual state.
KeywordsOxygen Methyl Ether Platinum Organic Chemistry
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