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Synthesis and characterization of poly-(methyl methacrylate-co-N-4-bromophenyl maleimide)

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Abstract

Radical copolymerization of methyl methacrylate (MMA, M1) and N-(4-bromophenyl) maleimide (N4BrPhMI, M2) in dioxane at 60 °C was performed with AIBN as initiator. Analysis of composition data points was carried out to a terminal model copolymerization. Using 1H, 13C and DEPT NMR measurements, the observed resonances were assigned. Glass transition temperatures were determined by DSC and a linear correlation was found between the Tg values and M2 content of the copolymers.

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Authors and Affiliations

  1. Department of Applied Chemistry, Kossuth L. University, H-4010, Debrecen, Hungary

    J. Borbély & T. Kelen

  2. Higher Pedagogical Institute, BG-9700, Shumen, Bulgaria

    V. B. Konsulov & Z. Grozeva

Authors
  1. J. Borbély
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  2. T. Kelen
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  3. V. B. Konsulov
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  4. Z. Grozeva
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Borbély, J., Kelen, T., Konsulov, V.B. et al. Synthesis and characterization of poly-(methyl methacrylate-co-N-4-bromophenyl maleimide). Polymer Bulletin 26, 253–258 (1991). https://doi.org/10.1007/BF00587966

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  • DOI: https://doi.org/10.1007/BF00587966

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