Summary
Mechanical, physical and chemical properties of ceramic materials are strongly dependent on the microstructure. Thus, the optimization of the microstructure plays a key role for a further improvement of advanced ceramics. The basis of microstructural optimization of ceramics is the relationship between processing, microstructure and properties. In these three fields, at present, extreme demands are put on microstructural characterization of ceramic materials. Microstructural characterization implies, besides the stereometric parameters, the analysis of the chemical composition and structure of the phases present in the material which in many cases have dimensions on an atomic level. In this paper the need for microanalytical characterization of advanced ceramics is pointed out from the materials point of view. Particularly, three topics are discussed:
-
problems and development lines in the field of advanced ceramics,
-
consequences for analytical investigations which are deduced from these problems, and
-
typical examples of analytical problems, and efforts to solve these problems by applying different analytical methods.
These topics will be discussed based on examples of highstrength and high-temperature ceramic materials, monolithic ceramics and ceramics composites.
Similar content being viewed by others
References
Ziegler G (1987) Metall 41:682–695
Abe H (1985) Am Ceram Soc Bull 64:1594–1596
Brook RJ (1986) In: Pask JA, Evans AG (eds) Ceramic microstructures '86, vol 21. Plenum Press, New York, pp 15–24
Wötting G, Ziegler G (1985) Ber Dtsch Keram Ges 1:33–42
Ziegler G (1987/88) Förderer des Bergbaus und des Hüttenwesens an der TU Berlin, Nr. 2 (1987), Nr. 1 (1988): 26–33
Menges G. Ziegler G (1988) Symposiumsband Materialforschung 1988 des BMFT, 12.–14. 9. 1988 in Hamm. Projektleitung Material- und Rohstofforschung (PLR) der KFA Jülich GmbH (Redakt.), pp 57–126
Ziegler G (1988) Symposiumsband Materialforschung 1988 des BMFT, 12.–14. 9. 1988 in Hamm. Projektleitung Material- und Rohstofforschung (PLR) der KFA Jülich GmbH (Redakt.), pp 765–786
Naslain PR (1985) In: Bunsell AR et al. (eds) Development in the science and technology of composite materials. 1st ECCM — 24.–27. 9. 1985, Bordeaux, France, pp 34–45
Clarke DR, Thomas G (1977) J Am Ceram Soc 60:491–495
Thomas G (1986) In: Pask JA, Evans AG (eds) Ceramic microstructures '86, vol 21. Plenum Press, New York, pp 55–72
Thonel A, Laval JY, Broussand D, Teste de Sagey G (1986) In: Pask JA, Evans AG (eds) Ceramic microstructures '86, vol 21. Plenum Press, New York, pp 263–270
Clarke DR (1987) Annu Rev Mater Sci 17:57–74
Wötting G, Ziegler G (1986) Powder Metal Int 18:305–313
Mecholsky JJ (1986) Am Ceram Soc Bull 65:315–322
Prewo KM, Brennan JJ, Layden GK (1986) Am Ceram Soc Bull 65:305–313
Tiegs TN, Becher PF, Harris LA (1986) In: Pask JA, Evans AG (eds) Ceramic microstructures '86, vol 21. Plenum Press, New York, pp 911–917
Dudek HJ, Braue PF, Ziegler G (1986/87) Ber Dtsch Keram Ges 2:3–20
Hausner H (1975) Sci Ceram 8:1–21
Rahaman MN, Boiteux Y, de Jonghe LC (1986) Am Ceram Soc Bull 65:1171–1176
Ijima S (1984) Jpn J Appl Phys 23:L347; J Electron Microsc 34:249–265
Braue W, Wötting G, Ziegler G (1986) Spec Ceram 8:71–80
Braue W, Dudek HJ, Ziegler G (1985) Mikrochim Acta 2:318–331
Thümmler F, Hamminger R, Gratwohl G (1986) Surf Interface Anal 8:453–462
Dudek HJ, Braue W, Ziegler G (1983) Mikrochim Acta 10:159–176
Braue W, Dudek HJ, Ziegler G (1983) In: Vincenzini P (ed) Ceramic powders. Elsevier, Amsterdam, pp 661–670
Lane JE, Carter GA, Davis RF (1988) J Am Ceram Soc 71:281–295
Braue W, Göring J, Ziegler G (1989) Proc 3rd Int Symp “Ceramic Components for Engine”, Las Vegas 1988 (in press)
Lewis MH, Barn P (1980) J Mater Sci 15:443–448
Nutt SR (1988) J Am Ceram Soc 71:149–156
Macey CJ, Lehmann RL, Moore RL (1984) Scanning Electron Microsc 1984:1643–1648
Braue W, Carpenter RW, Smith DJ (1989) Proc EMSA, Milwaukee, USA, 7.–12. 8. 1988 (in press)
Braue W, Hölscher A, Ziegler G (1988) Vortrag, Special Meeting, Tag Dtsch Keram Ges 19./20. 10. 1988, München
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Ziegler, G. Analytical problems with ceramic materials. Z. Anal. Chem. 333, 360–372 (1989). https://doi.org/10.1007/BF00572328
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF00572328