Skip to main content
Log in

A method for the preparation of PMMA-SiO2 nanocomposites with high homogeneity

  • Published:
Applied Composite Materials Aims and scope Submit manuscript

Abstract

It is possible to optimize the performance of the inorganic-organic composites dispersing the inorganic component in the organic matrix on a nanomiter length scale. If dry the inorganic phase cannot be intimately dispersed during the incorporation in the matrix. When the particle surface is organically modified, and the incorporation is made starting from a liquid dispersion (particles in polymer solution), the resulting composites exhibit an excellent homogeneity. Here, monolithic [poly(methyl methacrylate)/monodisperse silica particles] nanocomposites have been prepared and characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), dynamic light scattering (DLS), micro-hardness, and differential scanning calorimetry (DSC).

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Roy, R.,Mater. Sci. Res. 21, 1986, 25.

    Google Scholar 

  2. Gianelis, E. P.,JOM 4, 1992, 474.

    Google Scholar 

  3. Gleiter, H.,Adv. Mater. 4, 1992, 474.

    Google Scholar 

  4. Novak, B. M.,Adv. Mater. 5, 1993, 474.

    Google Scholar 

  5. Usuki, A., Kojima, Y., Kurauchi, T., Kamigaito, O., Kawosumi, M., Okada, A. and Fukushina, Y.,J. Mater. Res. 8, 1993, 1179.

    Google Scholar 

  6. Usuki, A., Kojima, Y., Kurauchi, T., Kamigaito, O., Kawosumi, M., Okada, A. and Fukushina, Y.,J. Mater. Res. 8, 1993, 1185.

    Google Scholar 

  7. Philipp, G. and Schmidt, H.,J. Non-Cryst. Solids 63, 1984, 283.

    Google Scholar 

  8. Schmidt, H., Krug, H., Kasemann, R. and Tiefensesee, F.,SPIE Submol. Glass Chem. Phys. 36, 1991, 1590.

    Google Scholar 

  9. Wang, M. S. and Pinnavaia, T. J.,Chem. Mater. 6, 1994, 468.

    Google Scholar 

  10. Lan, T. and Pinnavaia, T. J.,Chem. Mater. 6, 1994, 2216.

    Google Scholar 

  11. Yano, K.,J. Polym. Sci., Part A: Polym. Chem. 31, 1993, 2493.

    Google Scholar 

  12. Pope, E. J. A., Asami, M. and Mackenzie, J. D.,J. Mater. Res. 4, 1989, 1018.

    Google Scholar 

  13. Pope, E. J. A., Asami, M. and Mackenzie, D. J., inMulticomponent Ultrafine Microstructure, L. E. McCandlish, D. E. Polk, R. W. Siegel and G. H. Kear (eds), Mater. Res. Soc. Symp. Proc. 132, Pittsburgh, PA, 1989, p. 105.

  14. Giesche, H. and Matijevic, E.,J. Mater. Res. 9, 1994, 436.

    Google Scholar 

  15. Hsu, W. P., Rongchi, Y. and Matijevic, E.,Dye and Pigments 19, 1992, 179.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Carotenuto, G., Nicolais, L., Kuang, X. et al. A method for the preparation of PMMA-SiO2 nanocomposites with high homogeneity. Appl Compos Mater 2, 385–393 (1996). https://doi.org/10.1007/BF00564575

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00564575

Key words

Navigation