Abstract
The substructure and cleavage fracture in two types of polycrystalline B4C specimens are investigated. It is shown that in specimens hot-pressed below 2000°C twins in poreless grains are effective barriers for cleavage cracks. Cleavage fracture occurs in planes of the type {10\(\bar 1\)1}. There are twins and faceted pores in grains of specimens sintered below 2200°C. In these grains cleavage is along the twinning planes. Pores eliminate the effect of twins as crack stoppers.
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References
P. S. Kislyi, M. A. Kuzenkova, N. I. Bondaruk, et al., Boron Carbide [in Russian], Naukova Dumka, Kiev (1988).
C. Wood, “The transport properties of boron carbide prepared by different techniques,” in: Proc. 9th Int. Symp. on Boron, Borides and Related Compounds, Duisburg Univ., Gesmapt. Hochschule, Duisburg (1987), pp. 213–222.
J. D. R. Machinnon, “High resolution imaging of B4C microstructure.” in: Boron Rich Solids, Int. Conf. New York (1986), pp. 114–120.
N. V. Belov and M. V. Klassen-Neklyudova, “Nature of crystal failure,” Zh. Tekhn. Fiz.,38, No. 3, 265–278 (1948).
C. T. Forwood, “The work of fracture in crystals of sodium chloride containing cavities,” Phil. Mag.,17, No. 148, 657–667 (1968).
A. G. Evans and T. G. Langdon, Structural Ceramics [Russian translation], Metallurgiya, Moscow (1980).
B. Ram, USA Patent 4707312, “Method for producing ceramic articles of increased fracture toughness,” Publ. Nov. 17, 1987.
T. Mori, T. Suzuki, and T. Iseki, “Deformation by the stress-induced transport of helium bubbles in SiC,” J. Amer. Ceram. Soc.,75, No. 1, 237–239 (1992).
D. S. Russel, H. A. Harlan, and E. M. Robert, “Influence of induced porosity on the thermal shock characteristics of Al2O3,” Amer. Ceram. Soc. Bull.,55, No. 11, 979–982 (1976).
A. N. Pilyankevich and G. S. Oleinik, “Features of the failure of twinned silicon carbide crystals of cubic modification,” Poroshk. Metal., No. 6, 93–98 (1978).
K. H. G. Ashbee, “Defects in boron carbide after nbeutron irradiation,” Acta Metallurgica,19, No. 10, 1079–1085 (1971).
A. N. Pilyankevich, G. S. Oleinik, and N. F. Ostrovskaya, “Structure of failure in polycrystalline silicon carbide,” Dokl. Akad. Nauk UkrSSR, Ser. A, No. 11, 1038–1041 (1976).
K. H. G. Ashbee and C. K. H. Dubose, “Dislocation nodes in boron carbide with special reference to nonstoichiometry,” Acta Metallurgica,20, No. 2, 241–245 (1972).
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Institute of Materials Science, Ukrainian Academy of Sciences, Kiev. Translated from Poroshkovaya Metallurgiya, Nos. 9–10, pp. 12–17, September–October, 1995.
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Oleinik, G.S., Ostapchuk, T.V. Effect of pores on the cleavage of twinned boron carbide crystals. Powder Metall Met Ceram 34, 500–504 (1996). https://doi.org/10.1007/BF00559956
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DOI: https://doi.org/10.1007/BF00559956