Abstract
We have studied structural changes in the high-temperature B2-phase in a large single crystal at temperatures near the premartensitic transformation B2 → B19′. We are the first to observe an extra 1/2 (110) reflection in neutron diffraction patterns taken along the [110]B2 direction as the sample is cooled below 420 K, but still far from the martensite start temperature (Ms=180 K). This extra reflection heralds the formation of long-range order in atomic displacements with wave vectorq=(1/2±δ)[110]2Θ/a. Premartensitic diffraction effects (caused by the development and correlation of lattice waves of atomic displacements with wave vectorsq 1′≊2Θ/a[1/3, 1/3, 0] andq 1″≊2Θ/1[1/3, 1/3] that were clearly visible in this same single crystal before the martensitic transformation B2 → R, appeared at even lower temperatures with substantially lower intensities.
Similar content being viewed by others
References
A. I. Lotkov, Author's abstract, Doctoral Dissertation, Institute of Strength Physics and Materials Research, Tomsk (1992).
V. N. Khachin, V. G. Pushin, and V. V. Kondrat'ev, Titanium Nickelides. Structure and Properties [in Russian], Nauka, Moscow (1992).
G. M. Michal, P. Moine, and R. Sinclair, Acta. Met.,30, 125 (1982).
C. M. Hwang, M. Meichle, M. B. Salamon, and C. M. Wayman, Phil. Mag. A.,47, 9 (1983).
C. M. Hwang, M. Meichle, M. B. Salamon, and C. M. Wayman, Phil. Mag. A,47, 31 (1983).
R. Sinclair, P. Moine, G. M. Michal, Proc. Int. Conf. Solid — Solid Phase Transform., Pittsburg: Warrendalle, Pa. 1982, p. 1253.
P. Moine, E. Coo, and R. Sinclair, Scr. Met.,18, 1143 (1984).
V. G. Pushin, V. V. Kondrat'ev, and V. N. Khachin, Izv. Vuzov. Fizika, No. 5, 5 (1985).
S. F. Dubinin, A. I. Lotkov, S. G. Teploukhov, V. N. Grishkov, and V. P. Skorobogatov, Fiz. Met. Metalloved., No. 4, 111 (1992).
H. Tietze, M. Mullner, P. Silgert, and W. Assmus, J. Phys. F Met. Phys.,15, 263 (1985).
V. N. Grishkov and A. I. Lotkov, Fiz. Met. Metalloved.,11, 351 (1985).
S. F. Dubinin, S. G. Teploukhov, and Yu. A. Izyumov, Fiz. Met. Metalloved.,50, 1276 (1980).
P. Moine, J. Allain, and B. Renker, J. Phys. F Met. Phys.,14, 2517 (1984).
H. Tietze and M. Mullner, J. Phys. C Sol. Stat. Phys.,17, 1259 (1984).
Author information
Authors and Affiliations
Additional information
Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 1, pp. 56–61, January, 1995.
Rights and permissions
About this article
Cite this article
Dubinin, S.F., Lotkov, A.I., Teploukhov, S.G. et al. Neutron diffraction studies of the premartensitic transformation B2 → B19′ in Ti49Ni51 single crystals. Russ Phys J 38, 46–50 (1995). https://doi.org/10.1007/BF00559513
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF00559513