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A possibility of direct observation of residual styrene in crosslinked polyesters by solid state13C NMR methods

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Summary

The cross and direct polarization NMR in solid state was employed to study crosslinked polyesters. It was demonstrated that direct-polarization solid state NMR spectra provide an evidence for the presence of residual styrene. In cross-polarization solid state NMR experiment styrene is discriminated against due to its high mobility at ambient temperature.

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Author notes

  1. J. Grobelny

    Present address: Institute of Macromolecular Compounds, Russian Academy of Sciences, 199004, St. Petersburg, Russian Federation

Authors and Affiliations

  1. Institute of Polymer Chemistry, Polish Academy of Sciences, PL-41-800, Zabrze, Poland

    I. Zhukov & J. Grobelny

Authors
  1. I. Zhukov
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  2. J. Grobelny
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Zhukov, I., Grobelny, J. A possibility of direct observation of residual styrene in crosslinked polyesters by solid state13C NMR methods. Polymer Bulletin 29, 219–223 (1992). https://doi.org/10.1007/BF00558060

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  • DOI: https://doi.org/10.1007/BF00558060

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