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Preparation of polyacrylonitrile fibre by spinning into organic baths

  • Carbon And Other Heat Resistant Fibers, Composite Materials, And Use Of These In National Economy
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Fibre Chemistry Aims and scope

Conclusions

-- The spinning of polyacrylonitrile copolymers into organic baths containing dimethyl sulfoxide and isopropyl alcohol has been investigated. It has been found that the optimum DMSO:IPA ratio in the precipitation bath is 60:40% by wt..

-- It has been discovered that the strength of the spun yarn is higher the lower the jet stretch.

-- The effect of temperature on orientation stretch ratio has been studied. It has been shown that the optimum temperature for heat stretching of PAN yarn lies in the range 155–160°C.

-- The dimethyl sulfoxide content of yarn has been determined by technological transitions. In the final yarn it does not exceed 0.3–1.2% by wt.

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Literature cited

  1. Japanese Application 61-89328; 61-132631; 61-97477; 60-246821.

  2. Japanese Application 1-298217, 1-306619.

  3. Carbochain Synthetic Fibres, K. E. Perepelkin (ed.) [in Russian], Khimiya, Moscow (1973).

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  4. L. N. Matveeva, T. A. Romanova, T. V. Rybina, L. A. Kochorova, V. A. Medvedev, and A. T. Serkov, Khim. Volokna, No. 4, 61–62 (1989).

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VNIIPV. Translated from Khimicheskie Volokna, No. 3, pp. 15–16, May–June, 1991.

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Romanova, T.A., Medvedev, V.A., Kochorova, L.A. et al. Preparation of polyacrylonitrile fibre by spinning into organic baths. Fibre Chem 23, 161–163 (1992). https://doi.org/10.1007/BF00545851

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  • DOI: https://doi.org/10.1007/BF00545851

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