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5-Phenyl-1,3,4-thiadiazole and 5-phenyl-1,2,4-triazoline-3-thione as products of dehydrogenation of cyclic tautomeric forms of benzaldehyde thiosemicarbazone

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

5-Pkenyl-1,3,4-thiadiazole and 5-phenyl-1,4-triazoline-3-thione are produced from heterocyclic tautomeric forms of benzaldehyde thiosemicarbazone in the gas phase under conditions existing in a mass spectrometer, and also in the solid phase in the course of thermolysis.

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References

  1. J. A. Vliengenthart and J. F. C. Vliengenthart, Rec. Trav. Chim., 85, 1266 (1966).

    Google Scholar 

  2. Y. M. Sheikh, A. M. Duffield, and C. Djerassi, Org. Mass Spectrom., 1, 633 (1968).

    Google Scholar 

  3. G. J. Karabatsos, F. M. Vane, and R. A. Taller, J. Am. Chem. Soc., 86, 3351 (1964).

    Google Scholar 

  4. K. N. Zelenin, O. B. Kuznetsova, P. B. Terent'ev, V. N. Torocheshnikov, V. V. Lashin, andV. V. Alekseev, Khim. Geterotsikl. Soedin., No. 12 1689 (1992).

    Google Scholar 

  5. K. N. Zelenin, O. B. Kuznetsova, V. V. Alekseev (Alekseyev), P. B. Terent'ev, V. N. Torocheshnikov, and V. V. Ovcharenko, Tetrahedron, 49, 1257 (1993).

    Google Scholar 

  6. A. J. Blackman, and J. H. Bowie, Austr. J. Chem., 25, 335 (1972).

    Google Scholar 

  7. D. Libermann, M. Moyeux, A. Ronaix, J. Maillard, andL. Hengl, Bull. Soc. Chim. Fr., No. 10, 957 (1953).

    Google Scholar 

  8. M. Ohta, and T. Higashijima, J. Pharm. Soc. Jpn., 72, 376 (1952).

    Google Scholar 

  9. C.-F. Kröger, W. Sattler, and H. Beyer, Justus Liebigs Ann. Chem., 643, 128 (1961).

    Google Scholar 

  10. N. A. Klyuev, I. I. Grandberg, L. B. Dmitriev, and Yu. A. Larshin, Zh. Org. Khim., 15, 2274 (1979).

    Google Scholar 

  11. N. A. Klyuev, Yu. V. Shurukhin, I. I. Grandberg, V. A. Rusinov, V. A. Zyryanov, and I. Ya. Postovskii, Khim. Geterotsikl. Soedin., No. 2, 265 (1980).

    Google Scholar 

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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp. 1554–1560, November, 1993.

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Terent'ev, P.B., Lashin, V.V., Ovcharenko, V.V. et al. 5-Phenyl-1,3,4-thiadiazole and 5-phenyl-1,2,4-triazoline-3-thione as products of dehydrogenation of cyclic tautomeric forms of benzaldehyde thiosemicarbazone. Chem Heterocycl Compd 29, 1340–1346 (1993). https://doi.org/10.1007/BF00532037

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  • DOI: https://doi.org/10.1007/BF00532037

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