Chemistry of Heterocyclic Compounds

, Volume 27, Issue 12, pp 1365–1367 | Cite as

Synthesis and x-ray diffraction analysis of 1-methyl-5-(methoxycarbonylmethyl)-4,6-dioxa-1-azoniabicyclo[3.3.0]octane bromide

  • D. A. Tikhomirov
  • O. S. Slyadevskaya
  • A. F. Mishnev
  • A. V. Eremeev
Article
  • 23 Downloads

Abstract

The reaction of methyl bromopropiolate with diethanolmethylamine gave a quaternized 5-(methoxycarbonylmethyl)-4,6-dioxa-1-azabicyclo[3.3.0]octane, the structure and conformation of which were studied by x-ray diffraction analysis.

Keywords

Methyl Bromide Organic Chemistry Diffraction Analysis Octane 

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

Literature Cited

  1. 1.
    D. A. Tikhomirov, O. S. Parafilova, and A. V. Eremeev, Khim. Geterotsikl. Soedin., No. 3, 406 (1991).Google Scholar
  2. 2.
    H. Walther, L. Haase, H. Gross, B. Costisella, and I. Keitel, J. Prakt. Chem., 322, 902 (1980).Google Scholar
  3. 3.
    F. H. Allen, O. Kennard, D. G. Watson, L. Brammer, A. G. Orpen, and R. Taylor, J. Chem. Soc., Perkin Trans. 2, No. 1, 1 (1987).Google Scholar

Copyright information

© Plenum Publishing Corporation 1992

Authors and Affiliations

  • D. A. Tikhomirov
    • 1
  • O. S. Slyadevskaya
    • 1
  • A. F. Mishnev
    • 1
  • A. V. Eremeev
    • 1
  1. 1.Institute of Organic SynthesisLatvian Academy of SciencesRiga

Personalised recommendations