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Heterocyclic analogs of pleiadiene. 58. Thiocyanogenation of permidones. Synthesis of perimidone-6,7-disulfides

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

The thiocyanogenation of 1, 3-disubstituted perimidones gives good yields of their 6 (7)-monothiocyano and 6, 7-dithiocyano derivatives. Alkaline hydrolysis of these derivatives leads to the formation of the corresponding disulfides. The reduction of 1, 3-dimethylperimidone-6,7-disulfide is accompanied by the destruction of the disulfide bridge and may be used for the synthesis of 6,7-dialkylmercaptoperimidones.

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Authors and Affiliations

  1. M. A. Suslov Rostov State University, 344006, Rostov-on-Don

    V. N. Stepanova, A. A. Konstantinchenko & A. F. Pozharskii

  2. Scientific-Research Institute of Organic Chemistry, 344090, Rostov-on-Don

    V. N. Stepanova, A. A. Konstantinchenko & A. F. Pozharskii

Authors
  1. V. N. Stepanova
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  2. A. A. Konstantinchenko
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  3. A. F. Pozharskii
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Additional information

Communication 57, see ref. [1].

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp. 1493–1496, November, 1985.

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Stepanova, V.N., Konstantinchenko, A.A. & Pozharskii, A.F. Heterocyclic analogs of pleiadiene. 58. Thiocyanogenation of permidones. Synthesis of perimidone-6,7-disulfides. Chem Heterocycl Compd 21, 1230–1233 (1985). https://doi.org/10.1007/BF00515218

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  • DOI: https://doi.org/10.1007/BF00515218

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