Skip to main content
SpringerLink
Log in

Synthesis of 2-acylmethyl- and 2-acylmethylene-1,3-dithiolo[4,5-b]quinoxalines from α-acetylenic ketones

  • Published:
Chemistry of Heterocyclic Compounds Aims and scope

Abstract

A number of 2-acylmethyl-1,3-dithiolo[4,5-b]quinoxaline derivatives were synthesized on the basis of the reaction of α-acetylenic ketones with quinoxaline-2,3-dithiol in dimethyl sulfoxide (DMSO) in the presence of K2CO3. Their monohydrochlorides were obtained. A new series of 2-acylmethylene-1,3-dithiolo[4,5-b]quinoxalines was obtained by the reaction of 1-bromo-2-acylacetylenes with quinoxaline-2,3-dithiol in DMSO in the presence of triethylamine.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

Literature cited

  1. B. Holmberg, Ark. Kemi, 2, 567 (1950); Chem. Abstr., 46, 100 (1952).

    Google Scholar 

  2. F. Bohlmann and E. Bresinsky, Chem. Ber., 97, 2109 (1964).

    Google Scholar 

  3. V. N. Elokhina, A. S. Nakhmanovich, I. D. Kalikhman, N. P. Sokol'nikova, and M. G. Voronkov, Khim. Geterotsikl. Soedin., No. 10, 1328 (1975).

    Google Scholar 

  4. V. N. Elokhina, R. V. Karnaukhova, A. S. Nakhmanovich, I. D. Kalikhman, and M. G. Voronkov, Zh. Org. Khim., 15, 57 (1979).

    Google Scholar 

  5. K. Hideg, O. Hideg-Hankovszky, and P. Sohar, Chem. Ber., 107, 2079 (1974).

    Google Scholar 

  6. M. I. Rybinskaya, Zh. Vses. Khim. Ova., 12, 12 (1967).

    Google Scholar 

  7. S. I. Miller, C. E. Orzech, C. A. Welch, G. R. Zeigler, and J. I. Dichstein, J. Am. Chem. Soc., 84, 2020 (1962).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Irkutsk Institute of Organic Chemistry, Siberian Branch, Academy of Sciences of the USSR, 664033, Irkutsk

    A. S. Nakhmanovich, V. N. Elokhina, R. V. Karnaukhova, G. G. Skvortsova & I. D. Kalikhman

Authors
  1. A. S. Nakhmanovich
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. V. N. Elokhina
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. R. V. Karnaukhova
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. G. G. Skvortsova
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. I. D. Kalikhman
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp. 1489–1491, November, 1982.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Nakhmanovich, A.S., Elokhina, V.N., Karnaukhova, R.V. et al. Synthesis of 2-acylmethyl- and 2-acylmethylene-1,3-dithiolo[4,5-b]quinoxalines from α-acetylenic ketones. Chem Heterocycl Compd 18, 1154–1156 (1982). https://doi.org/10.1007/BF00506362

Download citation

  • Received:

  • Revised:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00506362

Keywords

Search

Navigation