Chemistry of Heterocyclic Compounds

, Volume 17, Issue 7, pp 719–722 | Cite as

Vibrational spectra and structure of 4-amino-1H-quinazolin-2-one 3-oxide

  • N. V. Abbakumova
  • A. F. Vasil'ev
  • E. B. Nazarova
Article
  • 26 Downloads

Abstract

On the basis of a study of the vibrational spectra in the solid state of the product of the reaction of 2-cyanophenyl isocyanate with hydroxylamine and its isotopic analogs (15N → O and 15NH2) it was demonstrated that the compound obtained has the 4-amino-1H-quinazolin-2-one 3-oxide structure.

Keywords

Organic Chemistry Solid State Isocyanate Hydroxylamine Vibrational Spectrum 

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Literature cited

  1. 1.
    N. V. Abbakumova, Yu. A. Baskakov, Yu. G. Putsykin, and L. D. Tomina, All-Union Institute of Scientific and Technical Information, Deposited Paper No. 239/74; Ref. Zh. Khim., 19N670 (1974).Google Scholar
  2. 2.
    L. Bellamy, Infrared Spectra of Complex Molecules, Methuen, London (1958).Google Scholar
  3. 3.
    H. Goncalves, F. Mathis, and C. Foulcher, Bull. Soc. Chim. Fr., No. 7, 2599 (1970).Google Scholar
  4. 4.
    D. I. Brown and K. Genaga, J. Chem. Soc., Perkin Trans. I, No. 21, 2182 (1975).Google Scholar
  5. 5.
    I. Hamer and A. Macaluso, Chem. Rev., 64, 474 (1964).Google Scholar
  6. 6.
    I. A. Grigor'ev, G. I. Shchukin, A. B. Dragunov, and L. B. Volodarskii, Izv. Sibirsk. Otd. Akad. Nauk SSSR, Ser. Khim. Nauk, 1, No. 2, 80 (1979).Google Scholar
  7. 7.
    A. Ya. Tikhonov and L. B. Volodarskii, Zh. Org. Khim., 9, 770 (1973).Google Scholar
  8. 8.
    V. A. Koptyug, L. B. Volodarskii, and I. K. Baeva, Zh. Obshch. Khim., 34, 151 (1964).Google Scholar
  9. 9.
    H. Gnichtel, R. Walentowski, and K. E. Schuster, Chem. Ber., 105, 1701 (1972).Google Scholar

Copyright information

© Plenum Publishing Corporation 1982

Authors and Affiliations

  • N. V. Abbakumova
    • 1
  • A. F. Vasil'ev
    • 1
  • E. B. Nazarova
    • 1
  1. 1.All-Union Scientific-Research Institute of Chemical Agents for the Protection of PlantsMoscow

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