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Synthesis of 3-acylmethyl-1,5-dihydrobenzo[e]-2,4-dithiepins and 1,2-di(acylvinylthiomethyl)-4,5-dimethylbenzenes from α-acetylene ketones

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

Substituted 1,5-dihydrobenzo[e]-2,4-dithiepins and 1,2-di(acylvinylthiomethyl)-4,5-dimethylbenzenes were synthesized by the reaction between α-acetylene ketones and 1,2-dimethyl-4,5-di(mercaptomethyl)benzene in chloroform in the presence of K2CO3 or in methanol in the presence of triethylamine.

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Literature cited

  1. A. S. Nakhmanovich, V. N. Blokhina, R. V. Karnaukhova, G. G. Skvortsova, and I. D. Kalikhman, Khim. Geterotsikl. Soedin., No. 11, 1489 (1982).

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Authors and Affiliations

  1. Irkutsk Institute of Organic Chemistry, Siberian Branch, Academy of Sciences of the USSR, 664033, Irkutsk

    A. S. Nakhmanovich, R. V. Karnaukhova, V. N. Elokhina & I. D. Kalikhman

Authors
  1. A. S. Nakhmanovich
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  2. R. V. Karnaukhova
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  3. V. N. Elokhina
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  4. I. D. Kalikhman
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 2, pp. 203–205, February, 1985.

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Nakhmanovich, A.S., Karnaukhova, R.V., Elokhina, V.N. et al. Synthesis of 3-acylmethyl-1,5-dihydrobenzo[e]-2,4-dithiepins and 1,2-di(acylvinylthiomethyl)-4,5-dimethylbenzenes from α-acetylene ketones. Chem Heterocycl Compd 21, 166–168 (1985). https://doi.org/10.1007/BF00504201

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  • DOI: https://doi.org/10.1007/BF00504201

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