Chemistry of Heterocyclic Compounds

, Volume 26, Issue 2, pp 201–203 | Cite as

Condensed imidazo-1,2,4-azines 22. Alkylation of 5H-imidazo[1,2-b]-1,2,4-triazepin-4-ones

  • V. P. Kruglenko
  • V. A. Idzikovskii
  • N. N. Kobets
  • M. V. Povstyanoi
Article
  • 21 Downloads

Abstract

Substituted 5H-imidazo[1,2-b]-1,2,4-triazepin-4-ones react with alkyl (alkenyl) halides, 2-chloroethanol, glycerin dichlorohydrin, haloacetic acids, the methyl ester and amide of monochloroacetic acid in a methanol-sodium methylate system to form N(5)-alkylation products, and with hydroxylamino-O-sulfonic acid to form 5-aminoimidazo[1,2-b]-1,2,4-triazepin-4-one.

Keywords

Methyl Ester Glycerin Organic Chemistry Amide 

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Literature Cited

  1. 1.
    V. P. Kruglenko, V. P. Gnidets, N. A. Klyuev, and M. V. Povstyanoi, Khim. Geterotsikl. Soedin., No. 8, 1109 (1989).Google Scholar
  2. 2.
    V. P. Kruglenko, N. S. Patalakha, P. B. Kurapov, N. A. Klyuev, V. A. Idzikovskii, I. I. Grandberg, and M. V. Povstyanoi, Khim. Geterotsikl. Soedin., No. 5, 694 (1985).Google Scholar
  3. 3.
    V. P. Kruglenko, V. A. Idzikovskii, N. A. Klyuev, and M. V. Povstyanoi, Khim. Geterotsikl. Soedin., No. 3, 386 (1988).Google Scholar
  4. 4.
    A. Gordon and R. Ford, A Chemists Guide [Russian translation], Mir, Moscow (1976).Google Scholar
  5. 5.
    Atlas of Mass Spectra [in Russian], No. 1, Izd. Novosibirsk. Inst. Khimii, Sib. Otd. Akad. Nauk SSSR, Novosibirsk (1977), No. 1, p. 27.Google Scholar
  6. 6.
    R. Wolkofs and S. Hammerun, Org. Mass Spectrom., 11, 375 (1976).Google Scholar
  7. 7.
    N. N. Kobets, V. P. Kruglenko, M. S. Kablova, and A. A. Timoshin, Ukr. Khim. Zh., 50, 1111 (1984).Google Scholar
  8. 8.
    N. A. Klyuev, V. Povstyanoi, G. G. Aleksandrov, and V. P. Gumennyi, Khim. Geterotsikl. Soedin., No. 1, 88 (1983).Google Scholar

Copyright information

© Plenum Publishing Corporation 1990

Authors and Affiliations

  • V. P. Kruglenko
    • 1
  • V. A. Idzikovskii
    • 1
  • N. N. Kobets
    • 1
  • M. V. Povstyanoi
    • 1
  1. 1.Kherson Industrial InstituteKherson

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