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Determination of the composition of hydrogenation products from nitrogenous heterocyclic compounds by gas chromatography-mass spectrometry

Bestimmung der Zusammensetzung der Hydrierungsprodukte heterocyclischer Stickstoffverbindungen durch GC-MS

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Zusammenfassung

Die Zusammensetzung der Produkte der Hochdruckhydrierung (MoS2-Katalysator) heterocyclischer Stickstoffverbindungen (Pyridin, Chinolin, Isochinolin, 2-Methylpyrrol), wie sie in Erdölfraktionen und ähnlichen Erzeugnissen vorkommen, wurde untersucht und diskutiert. Änderungen der Zusammensetzung in Abhängigkeit von der Temperatur wurden ebenfalls berücksichtigt.

Summary

The composition of the products of high-pressure hydrogenation on MoS2 catalyst of heterocyclic compounds (pyridine, quinoline, isoquinoline, 2-methylpyrrole) belonging to the types of compounds currently occurring in the fractions of petroleum and in similar products was determined by GC-MS. The change of composition of these products with different temperatures was investigated.

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Authors and Affiliations

  1. Laboratory of Synthetic Fuels, Institute of Chemical Technology, CS-166 28, Prague 6, ČSSR

    Z. Kafka, M. Kuraš, J. Novák & L. Vodička

Authors
  1. Z. Kafka
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  2. M. Kuraš
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  3. J. Novák
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  4. L. Vodička
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Kafka, Z., Kuraš, M., Novák, J. et al. Determination of the composition of hydrogenation products from nitrogenous heterocyclic compounds by gas chromatography-mass spectrometry. Z. Anal. Chem. 321, 475–478 (1985). https://doi.org/10.1007/BF00487084

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  • DOI: https://doi.org/10.1007/BF00487084

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