Abstract
High-dilution cycloacylation of 2-acetoxy-1,3-bis-(2-aminophenoxy)propane with the diacid chlorides of glutaric, diglycollic, thiodiglycollic, and N-tosyliminodiacetic acids gives the macrocyclic diamides. Subsequent reduction with boron hydride affords 16-membered dibenzodiaza-crown compounds.
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See [1] for communication 5.
Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 2, pp. 275–279, February, 1991.
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Formanovskii, A.A., Mikhura, I.V. Synthesis of macroheterocyclic analogs of dibenzo-crown compounds. 6. Hydroxylated 16-membered oxaaza-crown compounds. Chem Heterocycl Compd 27, 227–231 (1991). https://doi.org/10.1007/BF00476764
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DOI: https://doi.org/10.1007/BF00476764