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Elemental trace determinations in aluminium by enrichment onto activated carbon combined with direct current arc optical emission spectrography

Emissionspektroskopische Bestimmung von Spurenelementen in Aluminium mit Gleichstrom-Lichtbogen nach ihrer vorherigen Anreicherung an Aktivkohle

  • Original Papers
  • Trace Element Analysis
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Summary

A combined procedure including enrichment by adsorption onto activated carbon and direct current (dc) arc emission spectrography has been investigated for elemental determination. In order to obtain reproducible volatilization of the analyte in the dc arc, the activated carbon was mixed with graphite powder and the arc operated in an argon atmosphere. The procedure has been used to determine some trace impurities in high-purity aluminium metal. The analytical error in the concentration range of 10−3–10−5% was less than 10% and the relative standard deviation was below 12%.

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References

  1. Paksy L (1984) Spectrochim Acta 39 B:1449–1458

    Google Scholar 

  2. Grove EL (1978) Applied atomic spectroscopy, vol 2. Plenum Press, New York

    Google Scholar 

  3. Ehrlich E (1977) XX. Coll Spectrosc Int and 7th Int Conf Atomic Spectrosc, Invited Lectures II:5

    Google Scholar 

  4. Berndt H, Slavin W (1975) At Abs Newsl 17:109–112

    Google Scholar 

  5. Welz B (1985) Atomic absorption spectrometry. Verlag Chemie, Weinheim

    Google Scholar 

  6. Jackwerth E, Lohmar J, Wittler G (1973) Fresenius Z Anal Chem 266:1–8

    Google Scholar 

  7. Jackwerth E, Berndt H (1975) Anal Chim Acta 74:299–309

    Google Scholar 

  8. Berndt H, Jackwerth E, Kimura M (1977) Anal Chim Acta 93:45–52

    Google Scholar 

  9. Kimura M, Egawa S (1982) Talanta 29:329–331

    Google Scholar 

  10. Doğan M, ElÇi L (1984) Spectrochim Acta 39 B:1189–1194

    Google Scholar 

  11. Vanderborght BM, Van Grieken RE (1977) Anal Chem 49:311–316

    Google Scholar 

  12. Van der Sloot HA, Wals GD, Das HA (1977) Anal Chim Acta 90:193–200

    Google Scholar 

  13. Berndt H, Messerschmidt J, Alt F (1981) Fresenius Z Anal Chem 306:385–393

    Google Scholar 

  14. Marczenko M, Mojski M, Balcerzak M (1975) Microchimica Acta 1:539–547

    Google Scholar 

  15. Manova TG, Raginskaya LK, Pevtsov GA, Pavlova LA (1972) Anal Abstr 23:109

    Google Scholar 

  16. Doğan M, ElÇi L (1985) XXIV Colloquium Spectroscopicum Internationale, Garmisch-Partenkirchen

  17. Paksy L, Lakatos I (1983) Spectrochim Acta 38 B:1099–1114

    Google Scholar 

  18. Lakatos I, Paksy L (1974) Acta Chim Acad Sci Hung 81:31–41

    Google Scholar 

  19. Paksy L, Lakatos I (1979) Acta Chim Acad Sci Hung 99:347–354

    Google Scholar 

  20. Paksy L, Lakatos I (1979) Acta Chim Acad Sci Hung 99:355–362

    Google Scholar 

  21. ElÇi L (1986) PhD thesis, Hacettepe University, Ankara, Turkey

    Google Scholar 

  22. Pohl FA (1954) Fresenius Z Anal Chem 142:19–23

    Google Scholar 

  23. Boumans PWJW (1965) Theory of spectrochemical excitation. Hilger and Watts, London

    Google Scholar 

  24. Spindler DC (1961) Appl Spectrosc 15:20–25

    Google Scholar 

  25. Boumans PWJW, Maessen FJMS (1969) Spectrochim Acta 24 B:585–610

    Google Scholar 

  26. Svoboda V, Kleinmann I (1968) Anal Chem 40:1534–1540

    Google Scholar 

  27. Nedjalkova N, Krasnobaeva N, Vukanovic V (1985) Spectrochim Acta 40 B:1047–1057

    Google Scholar 

  28. Szoba ZL (1974) Spectrochim Acta 29 B:231–239

    Google Scholar 

  29. Vallee BL, Baker MR (1956) J Opt Soc Am 46:77–82

    Google Scholar 

  30. Stallwood BJ (1953) J Opt Soc Am 44:171–176

    Google Scholar 

  31. Emery RSJ (1952) Spectrochim Acta 4:513–515

    Google Scholar 

Download references

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Authors and Affiliations

  1. Fen-Edebiyat Fakültesi, Erciyes üniversitesi, Kayseri, Turkey

    L. ElÇi & M. Doĝan

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  1. L. ElÇi
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  2. M. Doĝan
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ElÇi, L., Doĝan, M. Elemental trace determinations in aluminium by enrichment onto activated carbon combined with direct current arc optical emission spectrography. Z. Anal. Chem. 330, 610–613 (1988). https://doi.org/10.1007/BF00473777

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  • DOI: https://doi.org/10.1007/BF00473777

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