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Hydroacridines and related compounds

XIII. 2-Phenyl-7,7-dimethyl-5h-7,8-dihydropyrano[4,3-b]pyridine: Synthesis and some of its transformations

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

2-Phenyl-7,7-dimethyl-5H-7,8-dihydropyrano[4,3-b]pyridine and its N-oxide were synthesized. Refluxing of the latter with acetic anhydride gives 2-phenyl-7,7-dimethyl-8-hydroxy-5H-7,8-dihydropyrano[4,3-b]pyridine acetate; hydrolysis of the acetate gives the alcohol.

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Literature cited

  1. G. A. Klimov, V. A. Stonik, and M. N. Tilichenko, Khim. Geterotsikl. Soedin., 821 (1973).

  2. G. A. Klimov, V. N. Ovsyannikova, and M. N. Tilichenko, Khim. Geterotsikl. Soedin., 1547 (1972).

  3. General Laboratory Manual for Organic Chemistry [Russian translation], Mir (1965), p. 450.

  4. A. N. Elizarova and I. N. Nazarov, Izv. Akad. Nauk SSSR, Otd. Khim. Nauk, 223 (1940).

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See [1] for communication XII.

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 6, pp. 824–825, June, 1973.

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Klimov, G.A., Krivenkova, A.V., Makar'eva, T.N. et al. Hydroacridines and related compounds. Chem Heterocycl Compd 9, 756–758 (1973). https://doi.org/10.1007/BF00472326

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  • DOI: https://doi.org/10.1007/BF00472326

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