Chemistry of Heterocyclic Compounds

, Volume 3, Issue 5, pp 647–649 | Cite as

3,3,3-Trifluoropropyl(methyl)cyclosiloxanes

I. Isolation and identification of trifluoropropyl(methyl)dimethylcyclosiloxanes
  • E. G. Kagan
  • Yu. A. Yuzhelevskii
  • A. L. Klebanskii
  • O. N. Larionova
  • A. V. Kharlamova
Article
  • 41 Downloads

Abstract

Mixtures of cyclosiloxanes containing 3, 3, 3-trifluoropropyl(methyl)-and dimethylcyclosiloxanes units, are separated by vacuum distillation and GLC. Three hitherto undescribed compounds are isolated and characterized. Six new cyclosiloxanes are identified by indirect methods in cuts which are mixtures. Chromatography and fractional distillation give results which are in satisfactory agreement.

Keywords

Methyl Chromatography Organic Chemistry Fractional Distillation Indirect Method 

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Reference

  1. 1.
    Yu. A. Yuzhelevskii, E. V. Kogan, and A. L. Klebanskii, ZhOKh, 33, 3773, 1963.Google Scholar
  2. 2.
    I. P. Yudina, Yu. A. Yuzhelevskii, and K. I. Sakodynskii, in collection: Gas Chromatography [in Russian], NIITEKhim, Moscow, 1965.Google Scholar
  3. 3.
    A. L. Klebanskii, Yu. A. Yuzhelevskii, E. V. Kogan, and E. G. Kagan, ZhOKh, 32, 323, 1962.Google Scholar

Copyright information

© The Faraday Press, Inc. 1969

Authors and Affiliations

  • E. G. Kagan
    • 1
  • Yu. A. Yuzhelevskii
    • 1
  • A. L. Klebanskii
    • 1
  • O. N. Larionova
    • 1
  • A. V. Kharlamova
    • 1
  1. 1.Lebedev All-Union Scientific Research Institute for Synthetic RubberLeningrad

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