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Fresenius' Zeitschrift für analytische Chemie

, Volume 330, Issue 8, pp 704–706 | Cite as

Determination of a metabolite of the herbicide Pyridate in plant extracts by MS/MS: recording of daughter spectra

  • J. Jaklin
  • P. Krenmayr
  • K. Varmuza
  • W. Heegemann
  • W. Landvoigt
Original Papers

Summary

A hybrid tandem mass spectrometer is used to determine the concentration of a herbicidal metabolite in plant extracts without any sample clean-up. A rather simple and quickly performable MS/MS-technique is applied with direct sample introduction, electron impact ionization and recording of daughter spectra. The reproducibility of the analysis is satisfactory; the limit of detection (10 ppm) is sufficient for screening if the plants have been sampled shortly after a spraying with the herbicide (coefficient of variation: 14%).

Keywords

Physical Chemistry Analytical Chemistry Inorganic Chemistry Mass Spectrometer Plant Extract 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Bestimmung eines Metaboliten des Herbicids Pyridate in Pflanzenextrakten mittels MS/MS: Aufnahme von Tochter-Ionen-Spektren

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References

  1. 1.
    Johnson J, Yost R (1985) Anal Chem 57:758 AGoogle Scholar
  2. 2.
    Schoen AE, Amy JW, Ciupek JD, Cooks RG, Dobberstein P, Jung G (1985) Int J Mass Spectrom Ion Processes 65:125Google Scholar
  3. 3.
    Huber JFK, Fogy I, Fioresi C (1980) Chromatographia 13:408Google Scholar
  4. 4.
    Lindner W, Ruckendorfer H (1983) Int J Environ Anal Chem 16:205Google Scholar
  5. 5.
    Mestres R, Susilo H, unpublishedGoogle Scholar
  6. 6.
    Bayzer H, Zohner A, unpublishedGoogle Scholar
  7. 7.
    Kováč J, Henselová M (1977) J Chromatogr 133:420Google Scholar
  8. 8.
    Landvoigt W, Malissa H Jr, Winsauer K (1982) Microchim Acta 1982 II:199Google Scholar
  9. 9.
    Malissa H Jr, Buchberger W, Landgraf E, Winsauer K (1984) Microchim Acta 1984 1:127Google Scholar

Copyright information

© Springer-Verlag 1988

Authors and Affiliations

  • J. Jaklin
    • 1
  • P. Krenmayr
    • 1
  • K. Varmuza
    • 1
  • W. Heegemann
    • 2
  • W. Landvoigt
    • 2
  1. 1.Institute for General ChemistryTechnical University ViennaViennaAustria
  2. 2.Chemie Linz AGLinzAustria

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