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The temperature field in rotational rheometers and flow curve correction for viscous dissipation

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Abstract

A solution is presented for incompressible non-Newtonian liquids of the one-dimensional stationary temperature field which arises due to heat dissipation between two concentric cylinders, the outer fixed and thermostated, the inner rotating at a constant angular velocity. The object of the study is to outline a simple procedure for determining the temperature rise of the liquid and, primarily, to ascertain the corrections of the consistent variables τ and D which enable the experimenter to rectify the rheogram on the basis of measurement of the shear stress τ and the angular velocity Ω. The results obtained are summarized in graphical form as diagrams of the temperature and velocity fields and, to facilitate practical application of the correction procedure, in a table relating the dimensionless temperature function Ψ(ℋ, n, ζ) to the geometry ℋ, the flow behaviour index n, and the coefficient of temperature rise ζ and showing the function Ψ′(1) as well.

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Abbreviations

a :

radius of the inner cylinder

b :

radius of the outer cylinder

Ω:

constant angular velocity of the inner cylinder

r*:

dimensionless radial coordinate r/b

ω*:

dimensionless angular velocity of the liquid

K :

fluid consistency index

n :

flow behaviour index

Θ:

dimensionless temperature rise (T−T 0)/T 0

T :

temperature of measured liquid (K)

T 0 :

temperature of the thermostated bath

Br:

Brinkman criterion

λf :

thermal conductivity of liquid

C :

constant of integration

β:

coefficient of sensitivity in consistency-temperature law

ε:

coefficient of sensitivity divided by flow behaviour index: β/n

Ψ(r*):

dimensionless temperature function

ζ:

coefficient of temperature rise; ζ=Br·ε

ℋ:

ratio of the radii of inner and outer cylinder

T(1):

temperature on the inner wall of the outer cylinder, i.e. for r*=1

δ:

outer cylinder wall thickness

α:

coefficient of heat transfer

q :

heat flux

k :

overall heat transfer coefficient

h :

height of measured liquid

λs :

thermal conductivity of the outer cylinder

Ψ′(1):

derivative of the dimensionless temperature function at point r*=1

γ:

dimensionless heat transfer constant

Ψ i (r*):

dimensional temperature function calculated for isothermal wall; T(1)=T 0

μ:

dynamic viscosity

Ψ i (ℋ):

maximum value of the dimensionless temperature function

Φ:

dimensionless symbol — ratio of C/C 0

D :

rate of shear

τ:

shear stress

\(\tilde D\) :

rate of shear (not considering dissipation)

\(\tilde \tau \) :

shear stress (not considering dissipation)

D + :

rate of shear corrected for the inner cylinder temperature

τ+ :

shear stress on the inner cylinder obtained by measurement on the rheometer used

\(\bar D\) j :

rate of shear on the inner cylinder for j-th measurement referred to a single constant temperature

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Štěpánek, A. The temperature field in rotational rheometers and flow curve correction for viscous dissipation. Applied Scientific Research 42, 15–31 (1985). https://doi.org/10.1007/BF00382528

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