Skip to main content
SpringerLink
Log in

Mechanochemical effects on the properties of starting mixtures for PbTiO3 ceramics by using a novel grinding equipment

  • Published:
Journal of Materials Science Aims and scope Submit manuscript

Abstract

The effects of milling were studied using a newly developed multi-ring media-type grinding machine on the synthesis processes of PbTiO3 ceramics from PbO-TiO2 mixed sols. The temperature of the endothermic and exothermic DTA peaks, corresponding to dehydration and crystallization, decreased with milling time. After milling the mixed sol for 5 min and heating to 823 K, the product was a single-phase PbTiO3. This suggests rapid homogenization and formation of lead titanate precursors during milling. The effects of milling were revealed to be much less when mixtures of dry and wet powders were used.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. S. Komatsubara, T. Isobe and M. Senna, J. Am. Ceram. Soc. 77 (1994) 278.

    Article  CAS  Google Scholar 

  2. K. Takeuchi, T. Isobe and M. Senna, J. Solid State Chem. 109 (1994) 401.

    Article  CAS  Google Scholar 

  3. M. Senna, Solid State Ionics 63–65 (1993) 3.

    Article  Google Scholar 

  4. Y. Kojima, T. Isobe, M. Senna, S. Ei-Escandarany K. Sumiyama and K. Suzuki, Int. J. Mechanochem. Mech. Alloying, 1 (1994) 32.

    CAS  Google Scholar 

  5. J. Liao and M. Senna, Solid State Ionics 66 (1993) 313.

    Article  CAS  Google Scholar 

  6. Y. Okamoto, T. Isobe and M. Senna, J. Non-Cryst. Solids 180 (1995) 171.

    Article  CAS  Google Scholar 

  7. K. Hamada and M. Senna, Kagaku Kogaku Ronbunshu 21 (1995) 334.

    Article  CAS  Google Scholar 

  8. K. Kubo, J. Soc. Powder. Technol. Jpn 15 (1978) 17.

    Google Scholar 

  9. J. M. Longo and K. C. Voight, Solid State Ionics 32/33 (1989) 409.

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Nara Machinery Co., Ltd, Jonan-jima Ohta-ku, 143, Tokyo, Japan

    K. Hamada

  2. Faculty of Science and Technology, Keio University, 223, Hiyoshi yokohama, Japan

    M. Senna

Authors
  1. K. Hamada
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. M. Senna
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Hamada, K., Senna, M. Mechanochemical effects on the properties of starting mixtures for PbTiO3 ceramics by using a novel grinding equipment. Journal of Materials Science 31, 1725–1728 (1996). https://doi.org/10.1007/BF00372184

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00372184

Keywords

Search

Navigation