Skip to main content
Log in

Curved crystal analysis using a triple-crystal X-ray spectrometer

  • Solids and Materials
  • Published:
Applied Physics A Aims and scope Submit manuscript

Abstract

A Bragg crystal spectrometer using cylindrically curved crystals is designed to focus a divergent X-ray beam. The spectral resolution and precision of focus is determined by the quality of the concavely curved crystal. The analysis of the quality of the crystal was done using a triplecrystal X-ray spectrometer, comparing parallel and antiparallel X-ray scans of the third curved crystal, determining flaws resulting from the bend. Topics discussed include the derivation of the crystal's quality, conditions of alignment for the Bragg reflection, and X-ray beam width contributions to the FWHM. Organic and inorganic crystals with varying values of Bragg angles are used.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Kazuyuki Tohji, Yasuo Udagawa, Tsutomu Kawasaki, Kimitoshi Mieno: Rev. Sci. Instrum. 59, 1127 (1988)

    Google Scholar 

  2. Tadashi Matsushita, Hiro-O Hashizume: X-Ray Monochromators. In Handbook on Synchrotron Radiation, Vol. 1, 261 (1983)

    Google Scholar 

  3. A.K. Freund: X-Ray Optics. In European Synchrotron Radiation Facility, ESRF internal report, Part 1 (July 1987)

  4. B.D. Cullity: Elements of X-Ray Diffraction (Addison-Wesley, Reading 1967)

    Google Scholar 

  5. A.E. Sandstrom: Experimental Methods of X-Ray Spectroscopy: Ordinary Wavelengths, in Encyclopedia of Physics Vol. 30, X-Rays (Springer, Berlin, Heidelberg 1957)

    Google Scholar 

  6. R.W. James: Optical Principles of the Diffraction of X-Rays. In Crystalline State Vol. II (Cornell University Press, New York 1965)

    Google Scholar 

  7. A.H. Cottrell: Dislocations and Plastic Flow in Crystals (Clarendon, Oxford 1953)

    Google Scholar 

  8. J. Friedel: Dislocations (Pergamon, Oxford 1964)

    Google Scholar 

  9. M.B. Hakim, W.S. Muney, W.B. Fowler, B.E. Woodgate: Proc. SPIE 982, 394 (1988)

    Google Scholar 

  10. V.F. Miuskov: In Plasticity of Crystals, ed. by M.V. Klassen-Neklyudova (Consultants Bureau, New York 1962)

    Google Scholar 

  11. J.W.M. Dumond: Phys. Rev. 52, 872 (1937)

    Google Scholar 

  12. R. Bubakova: Czech. J. Phys. B 12, 776 (1962)

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Hakim, M.B., Woodgate, B.E. Curved crystal analysis using a triple-crystal X-ray spectrometer. Appl. Phys. A 51, 369–373 (1990). https://doi.org/10.1007/BF00348374

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00348374

PACS

Navigation