Abstract
A method for the analyses of pyridine in environmental samples is described. For soil samples a distillation procedure followed by an extraction, an acidic extraction or a Soxhlet extraction can be used. For water samples a distillation procedure followed by extraction can be employed. Deuterated pyridine is used as an internal standard and the extracts are analyzed by GC-MS. The recoveries of the methods are higher than 80%; the detection limits for pyridine are 0.01 mg/kg for soil samples and 0.2 μg/l for water samples.
References
Tsukioka T, Murakami T (1987) J Chromatogr 396:319
Macák J, Nabivach V, Buryan P, Berlizov JS (1981) J Chromatogr 209:472
Richard JJ, Junk GA (1984) Anal Chem 56:1625
Novotny M, Kump R, Merli F, Todd L (1980) J Anal Chem 52:401
Felice L (1982) J Anal Chem 54:869
Kaczvinsky JR, Saitoh K, Fritz JS (1983) Anal Chem 55:1210
Stuber HA, Leenheer JA (1983) Anal Chem 55:111
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Peters, R.J.B., van Renesse van Duivenbode, J.A.D. Determination of pyridine in soil and water samples of a polluted area. Fresenius J Anal Chem 348, 249–251 (1994). https://doi.org/10.1007/BF00325369
Received:
Revised:
Issue Date:
DOI: https://doi.org/10.1007/BF00325369