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Solid state analysis in mechanochemistry by high resolution 27Al solid state NMR spectroscopy

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Abstract

Modern solid state NMR techniques [one-dimensional magic angle spinning (MAS) and two-dimensional quadrupole nutation experiments with MAS] are applied for the characterization of mechanochemically activated inorganic powders such as hydrargillite [γ-Al(OH)3] and pseudo-boehmite [synthetic γ-AlO(OH)]. The materials were activated in a vibration mill.

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Authors and Affiliations

  1. Federal Institute for Materials Research and Testing, Rudower Chaussee 5, D-12489, Berlin, Germany

    Werner Storek

  2. Centre of Heterogeneous Catalysis, Rudower Chaussee 5, D-12489, Berlin, Germany

    Hendrik Kosslick & Vu Anh Tuan

  3. WITEGA-Research GmbH, Rudower Chaussee 5, D-12489, Berlin, Germany

    Hans-Peter Hennig

Authors
  1. Werner Storek
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  2. Hendrik Kosslick
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  3. Vu Anh Tuan
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  4. Hans-Peter Hennig
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Storek, W., Kosslick, H., Tuan, V.A. et al. Solid state analysis in mechanochemistry by high resolution 27Al solid state NMR spectroscopy. Fresenius J Anal Chem 349, 225–227 (1994). https://doi.org/10.1007/BF00323286

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  • DOI: https://doi.org/10.1007/BF00323286

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