Skip to main content
SpringerLink
Log in

Direct solid sample analysis of SiC-powders by DC glow discharge and DC-ARC emission spectroscopy

  • Short Communications
  • Published:
Fresenius' Journal of Analytical Chemistry Aims and scope Submit manuscript

Abstract

Glow discharge atomic emission spectroscopy (GD-OES) and the classical spectrographic method with a dc arc source (DC-ARC OES) have been applied to the direct analysis of SiC powders. The homogeneity of pellets prepared from mixtures of SiC with copper powder and used for the GD experiments was investigated in detail. Various methods have been tested for the analytical calibration. These have been applied to the direct solid sample analysis of technical SiC powders. The experimental data were evaluated by chemometrical procedures. The results of the two methods have been compared.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

References

  1. Broekaert JAC, Tölg G (1990) Mikrochim Acta (Wien) II:173–188

    Google Scholar 

  2. Ehrlich G, Stahlberg U, Hoffmann V (1992) Spectrochim Acta 46B:115–124

    Google Scholar 

  3. Flórián K, Nickel H, Zadgorska Z (1993) Fresenius J Anal Chem 345:445–450

    Google Scholar 

  4. Hassler J, private communication of Elektroschmelzwerk, Kempten/Germany

  5. Guntur DS, Fischer W, Mazurkiewicz M, Naoumidis A, Nickel H (1992) Reports of the Research Centre Jülich, Jül-Report No. 2592

  6. Nickel H, Zadgorska Z, Wolff G (1993) Spectrochim Acta 48B:25–38

    Google Scholar 

  7. Zimmer K, Heltai G, Flórián K (1982) Evaluation of emission spectra. In: Progr Anal At Spectrosc 5:341–467

    Google Scholar 

  8. Fischer W, Naoumidis A, Nickel H (1994) J Anal At Spectrom (in press)

  9. Flórián K, Fischer W, Hassler J, Nickel H (1993) XXXVIth Hungarian Annual Conference on Spectral Analysis, Lilafüred/Hungary, August 24–27, 1993, Proc, p 99–104

Download references

Author information

Authors and Affiliations

  1. Department of Chemistry, TU Kosice, Letná 9, SK-04200, Kosice, Slovakia

    K. Flórián

  2. Institute for Materials in Energy Systems, Research Centre Jülich GmbH, P. O. Box 1913, D-52425, Jülich, Germany

    W. Fischer & H. Nickel

Authors
  1. K. Flórián
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. W. Fischer
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. H. Nickel
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Flórián, K., Fischer, W. & Nickel, H. Direct solid sample analysis of SiC-powders by DC glow discharge and DC-ARC emission spectroscopy. Fresenius J Anal Chem 349, 174–175 (1994). https://doi.org/10.1007/BF00323259

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00323259

Keywords

Search

Navigation