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Preparation of the bovine liver 12-02-01 reference material and the certification of element contents from an interlaboratory comparison

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Summary

The preparation of the bovine liver 12-02-01 reference material, its stabilization and homogeneity testing is presented. Evaluation of an interlaboratory comparison in which 31 laboratories took part using several analytical methods is described. From the results of the intercomparison, the contents of the elements Cd, Cu, Hg, Mn, Pb, Se, and Zn were certified, while for the elements Br, Co, Fe, K, Mo, Na, and Rb, information values were derived. Non-recommended values for the elements Ag, As, Ca, Cl, Cr, Cs, La, Mg, S, Sb, Sn, Sr, and V were also evaluated.

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References

  1. Muramatsu Y, Parr RM (1985) Survey of currently available reference materials for use in connection with the determination of trace elements in biological and environmental materials. IAEA/RL/128, Vienna

    Google Scholar 

  2. Gladney ES, O'Malley BT, Roelandts I, Gills TE (1987) Standard reference materials: compilation of elemental concentrations data for NBS clinical, biological, geological, and environmental standard reference materials. NBS Spec. Pub, p 260–111, Gaithersburg

    Google Scholar 

  3. Wagstaffe PJ, Hecht H, Muntau H, Schramel P (1987) Fresenius Z Anal Chem 329:475

    Google Scholar 

  4. Mader P, Kučera J, Cibulka J, Miholová D (1989) Chem Listy 83:765

    Google Scholar 

  5. Kučera J, Soukal L (1988) J Radioanal Nucl Chem Articles 121:245

    Google Scholar 

  6. Kučera J, Mader P, Miholová D, Cibulka J, Poláková M, Kordík K (1989) Report on the interlaboratory comparison of the determination of the content of trace elements in bovine liver 12-02-01, Czechoslovak Institute of Metrology, Bratislava

    Google Scholar 

  7. Püschel P, Formánek Z, Vlasáková, Stuchlíková A (1988) Proc. 3th Czechoslovak Spectroscopic Conference, České Budějovice, June 19–24

  8. Püschel P, Formánek Z, Vlasáková A, Stuchlíková A (1988) Proc X. CANAS, September 5–9

  9. Trace mercury analyzer TMA 254, information leaflet, the science and research section of the Prague institute of chemical technology, Prague

  10. Hlaváč R, Doležal J, Kolihová D, Sychra V, Pietroš L, Valenta S, Püschel P, Formánek Z (1985) Proc. XIV CSI, Garmisch-Partenkirchen, September

  11. Dybczynski R (1980) J Radioanal Chem 60:45

    Google Scholar 

  12. Kučera J (1989) Radioisotopy 30:195

    Google Scholar 

  13. Eckschlager K, Horsák I, Kodejš Z (1980) Vyhodnocování analytických výsledk∪ a metod. SNTL, Praha

    Google Scholar 

  14. Shapiro SS, Wilk MB (1965) Biometrika 52:591

    Google Scholar 

  15. Dybczynski R (1980) Anal Chim Acta 117:53

    Google Scholar 

  16. Davies PL (1988) Fresenius Z Anal Chem 331:513

    Google Scholar 

  17. Sachs L (1982) Applied statistics, a handbook of techniques. Springer, Berlin Heidelberg New York

    Google Scholar 

  18. Griepink B, Colinet E, Gonska H, Muntau H (1984) Report EUR 9251 EN, Community Bureau of Reference. CEC, Brussels

    Google Scholar 

  19. Marchandise H, Colinet E (1983) Fresenius Z Anal Chem 316:669

    Google Scholar 

  20. Certificate of analysis for standard reference material 1577, bovine liver (1977) NBS, Washington, Revision 14 June

  21. Certificate of analysis of standard reference material 1577a, bovine liver (1985) NBS, Gaithersburg, February

  22. Czechoslovak state norm (1964) ČSN 01 2801, Vydavatelství ÚNM, Prague

  23. Toro EC, Parr RM, Clements SA (1990) IAEA/RL/128 (RV.1), Vienna

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Authors and Affiliations

  1. Nuclear Research Institute, CS-250 68, Řež near Prague, ČSFR

    J. Kučera

  2. Agronomical Faculty, Trace Element Laboratory, University of Agriculture, CS-165 21, Prague 6 — Suchdol, ČSFR

    P. Mader, D. Miholová & J. Cibulka

  3. Czechoslovak Institute of Metrology, L. Novomeského IV/487, CS-842 55, Bratislava, ČSFR

    M. Poláková & D. Kordík

Authors
  1. J. Kučera
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  2. P. Mader
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  3. D. Miholová
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  4. J. Cibulka
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  5. M. Poláková
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  6. D. Kordík
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Additional information

Denoted as CZIM-liver in the report [23]

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Kučera, J., Mader, P., Miholová, D. et al. Preparation of the bovine liver 12-02-01 reference material and the certification of element contents from an interlaboratory comparison. Fresenius J Anal Chem 338, 66–71 (1990). https://doi.org/10.1007/BF00322788

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  • DOI: https://doi.org/10.1007/BF00322788

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