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Frequency-modulated simultaneous multielement atomic absorption spectrometry using electrothermal atomizer and deuterium background correction

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Abstract

Characteristic data of the frequency-modulated simultaneous multielement atomic absorption spectrometry (FREMSAAS) using electrothermal atomizer with deuterium background correction, have been determined. The data obtained have been processed by using several statistical tests recommended for quality control purposes. The instrumentation has been presented as well as procedures of separating elements into measure groups and fixing of variable conditions. Detection limits, characteristic masses and working ranges have been given for the eleven elements examined. The data have been in good agreement to results obtained with conventional one-channel AAS instruments. The eleven elements have been simultaneously determined in a standard reference material (SRM) and all results are compatible with a 95% certainty with the certified values. FREMSAAS has been applied to a real sample.

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Authors and Affiliations

  1. Chair of Analytical Chemistry, Institut für Chemo- und Biosensorik e.V., Westfälische Wilhelms-Universität, Mendelstrasse 7, D-48149, Münster, Germany

    H. Edel, L. Quick & K. Cammann

Authors
  1. H. Edel
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  2. L. Quick
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  3. K. Cammann
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Dedicated to Professor Dr. Dieter-Klockow on the occasion of his 60th birthday

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Edel, H., Quick, L. & Cammann, K. Frequency-modulated simultaneous multielement atomic absorption spectrometry using electrothermal atomizer and deuterium background correction. Fresenius J Anal Chem 351, 479–483 (1995). https://doi.org/10.1007/BF00322719

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  • DOI: https://doi.org/10.1007/BF00322719

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