Summary
The reduction of syndiotactic or isotactic polymethyl-methacrylate yields the tactic polymethallylalcohols. Degree of conversion and tacticity can be determined by 1H-and 13C-NMR. The polymethallylalcohols are reacted with isocyanates to obtain the corresponding polymethallyl urethanes whose 13C-NMR spectra are also studied.
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Lenk, H., Klesper, E. 1H- and 13C-NMR of tactic polymethallylalcohols and polymethallylurethanes. Polymer Bulletin 3, 513–520 (1980). https://doi.org/10.1007/BF00256293
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DOI: https://doi.org/10.1007/BF00256293