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Extraction and recovery of asphalt binder: a literature review

  • Peter MikhailenkoEmail author
  • Parinaz Ataeian
  • Hassan Baaj
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Abstract

A literature review was conducted on the main aspects of asphalt binder extraction and recovery: i) extraction methods, ii) recovery methods and iii) solvents. The extraction methods include centrifuge, reflux and vacuum and others with particular focus on their effectiveness in dissolving the binder and the potential to modify it. Studies found that the centrifuge was a relatively safe cold extraction method that was fairly effective. For the recovery methods, the rotary evaporator was found to have a good reputation for relative ease of use and less binder modification than for the Abson method. The most commonly used solvents n-propyl bromide and chlorinated solvents, while being reusable, both had reported issues of ineffectiveness as well as major concerns about user safety. Bio-sourced solvents were found to be seldom used and required higher quantities. The study concluded that more research needed to be done in developing solvents.

Keywords

Asphalt binder testing Extraction Recovery Solvent RAP 

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Notes

Acknowledgements

The authors would like to thank Imran Bashir and Pamela Marks of Ministry of Transportation Ontario (MTO) for their support during the project and their valuable feedback. This project was funded as part of the MTO HIIFP 2015 Program.

References

  1. [1]
    American Association of State Highway and Transportation Officials, Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR). AASHTO T 315. Washington DC, USA, 2017.Google Scholar
  2. [2]
    American Society for Testing and Materials, Standard Test Method for Softening Point of Bitumen (Ring-and-Ball Apparatus). ASTM D 46. West Conshohocken, PA, USA, 2014.Google Scholar
  3. [3]
    American Society for Testing and Materials, Standard Test Method for Penetration of Bituminous Materials. ASTM D 5. West Conshohocken, PA, USA, 2013.Google Scholar
  4. [4]
    American Association of State Highway and Transportation Officials, Determining the flexural creep stiffness of asphalt binder using the bending beam rheometer (BBR). AASHTO T 313. Washington DC, USA, 2017.Google Scholar
  5. [5]
    J. Huet, Recovery method with rotary evaporator of the soluble binder from bituminous mixes: interlaboratory test comparisons and test procedure recommendation, Mater. Struct. 21(2) (1988) 151–160.Google Scholar
  6. [6]
    M. Zargar, E. Ahmadinia, H. Asli, M.R. Karim, Investigation of the possibility of using waste cooking oil as a rejuvenating agent for aged bitumen, J. Hazard. Mater. 233-234 (2012) 254–258.Google Scholar
  7. [7]
    A. Copeland, Reclaimed asphalt pavement in asphalt mixtures: state of the practice. No. FHWA-HRT-11-021. Federal Highway Administration, Washington DC, 2011.Google Scholar
  8. [8]
    I.L. Al-Qadi, M. Elseifi, S.H. Carpenter, Reclaimed Asphalt Pavement–A Literature Review. FHWA-ICT-07-001. Illinois Center for Transportation, Urbana, IL, 2007.Google Scholar
  9. [9]
    T. Baghaee Moghaddam, H. Baaj, The use of rejuvenating agents in production of recycled hot mix asphalt: A systematic review, Constr. Buil. Mater. 114 (2016) 805–816.Google Scholar
  10. [10]
    B. Huang, G. Li, D. Vukosavljevic, X. Shu, B. Egan, Laboratory investigation of mixing hot-mix asphalt with reclaimed asphalt pavement, Transp. Res. Rec. 1929(1) (2005) 37–45.Google Scholar
  11. [11]
    A. Monterpara, F. Giuliani, Control of binder content in bituminous mixes by means of an automatic apparatus, in: TRANSCOM ’99, Zilina, Slovakia, 1999.Google Scholar
  12. [12]
    N. Piérard, S. Vansteenkiste, A. Vanelstraete, Effect of Extraction and Recovery Procedure on the Determination of PmB Content and on the Properties of the Recovered Binder, Road Mater. Pave. Des. 11 (sup 1) (2010) 251–279.Google Scholar
  13. [13]
    S. Kim, T. Byron, G.A. Sholar, J. Kim, Evaluation of Use of High Percentage of Reclaimed Asphalt Pavement (RAP) for Superpave Mixtures. DOT/SMO/07-507. State Materials Office, Florida Department of Transportation, Florida, USA, 2007.Google Scholar
  14. [14]
    E.R. Brown, N.E. Murphy, S. Mager, L. Yu, Historical development of asphalt content determination by the ignition method, Asphalt Paving Technol. 64 (1995) 241–277.Google Scholar
  15. [15]
    M.S. Sondag, B.A. Chadbourn, A. Drescher, Investigation of Recycled Asphalt Pavement (RAP) Mixtures, University of Minnesota, Minneapolis, MN, 2002.Google Scholar
  16. [16]
    B.L. Burr, R.R. Davison, H.B. Jemison, C.J. Glover, J.A. Bullin, Asphalt Hardening in Extraction Solvents, Transp. Res. Rec. 1323 (1991) 70–76.Google Scholar
  17. [17]
    R.L. Peterson, H.R. Soleymani, R.M. Anderson, R.S. McDaniel, Recovery and Testing of RAP Binders from Recycled Asphalt Pavements, in: 78th Annual Meeting of the Transp. Res. Board, Washington, DC, 1999.Google Scholar
  18. [18]
    S.D. Diefenderfer, Developing a Laboratory Protocol for Asphalt Binder Recovery. FHWA/VCTIR 15-R7. Virginia Center for Transportation Innovation and Research, Virginia, USA, 2014.Google Scholar
  19. [19]
    N. Piérard, A. Vanelstraete, Quid de la mesure de la teneur en liant par extraction au solvant dans le cas des liants bitumineux modifiés aux polymères et des liants pigmentables [On the measurement of the binder content by solvent of polymer modified and pigmented bitumen], in: Congrès Belge de La Route, Liege, Belgium, 2013.Google Scholar
  20. [20]
    H. Baaj, P. Dorchies, D. Perraton, B. Tessier, Module complexe et comportement à basse température des enrobés bitumineux modifiés aux bardeaux d’asphalte [Complex modulus and low-temperature behavior of asphalt mixtures modified with asphalt shingles], in: Proceedings of the Canadian Technical Asphalt Association Conference, Montreal, Quebec, Canada, 2004 pp. 315–240.Google Scholar
  21. [21]
    D. Swiertz, E. Mahmoud, H. Bahia, Estimating the effect of recycled asphalt pavements and asphalt shingles on fresh binder, low-temperature properties without extraction and recovery, Transp. Res. Rec. 2208(1) (2011) 48–55.Google Scholar
  22. [22]
    O. Sirin, M. Tia, Investigation of problems in binder extraction from conventional and rubber modified asphalt mixtures, in: Sixth International RILEM Symposium on Performance Testing and Evaluation of Bituminous Materials, RILEM Publications SARL, Zurich, Switzerland, 2003, pp. 212–219.Google Scholar
  23. [23]
    D. Bechtel, A Short Review of 1-Bromopropane Literature and Contrast to Trichloroethylene Use in Aggregate Analysis, PRTox Consulting Inc., Saskatoon, Saskatchewan, Canada, 2012.Google Scholar
  24. [24]
    A. Andriescu, T. Arnold, N. Gibson, A. Shastry, S. Needham, S. Parobeck, Development of an Asphalt Binder Solvent Recovery Method as an Alternative to Rotovapor ASTM D 5404, FHWA Turner-Fairbank Highway Research Center, McLean, Virginia, USA, 2016.Google Scholar
  25. [25]
    G.W. Steele, F.L. Krieger, Statistical Evaluation of Equipment and Operator Effects on the Results of Asphalt Extraction Tests, in: Assoc Asphalt Paving Technol Proc, Denver, Colorado, USA, 1967.Google Scholar
  26. [26]
    American Society for Testing and Materials, Quantitative Extraction of Bitumen from Bituminous Paving Mixtures. ASTM D 2172, West Conshohocken, PA, USA, 2011.Google Scholar
  27. [27]
    A. Norton Jr, High Reclaimed Asphalt Pavement in hot mix asphalt, (Master Thesis), Rowan University, NJ, USA, 2012.Google Scholar
  28. [28]
    P. Mikhailenko, H. Baaj, Survey of Current Asphalt Binder Extraction and Recovery Practices, in: 2017 Transportation Association of Canada Conference, St. John’s, Canada, 2017.Google Scholar
  29. [29]
    European Committee for Standardization (CEN), Bituminous mixtures. Test methods for hot mix asphalt. Soluble binder content. EN 12697-1. Brussels, Belgium, 2012.Google Scholar
  30. [30]
    American Association of State Highway and Transportation Officials, Standard Method of Test for Quantitative Extraction of Asphalt Binder from Hot Mix Asphalt (HMA). AASHTO T 164, Washington DC, USA, 2014.Google Scholar
  31. [31]
    American Society for Testing and Materials, Standard Test Method for Recovery of Asphalt From Solution by Abson Method. ASTM D 1856. West Conshohocken, PA, USA, 2009.Google Scholar
  32. [32]
    D.E. Carey, H.R. Paul, Evaluation of asphalt cement extraction and recovery methods. Research Report No. 157. Louisiana Department of Transportation, Louisiana, USA, 1982.Google Scholar
  33. [33]
    M. Stroup-Gardiner, J.W. Nelson, Use of normal propyl bromide solvents for extraction and recovery of asphalt cements. Report No. NCAT 6. National Center for Asphalt Technology, Auburn, AL, USA, 2000.Google Scholar
  34. [34]
    Y. Mehta, A. Nolan, S. Coffey, Eric Du Bois, A. Norton, D. Reger, P. Shirodkar, K. Sonpal, C. Tomlinson, High Reclaimed Asphalt Pavement In Hot Mix Asphalt. No. FHWA-NJ-2012-005. Rowan University, Washington DC, 2012.Google Scholar
  35. [35]
    N. Piérard, Quid de l’extraction et de la récupération des liants modifiés au polymère d’enrobés bitumineux? Les procédures classiques sont-elles toujours applicables? [On the extraction and recovery of polymer modified and bitumen? Are the classic procedures still applicable?], Bulletin CRR., 2011, p. 12–16.Google Scholar
  36. [36]
    S. Varamini, S.L. Tighe, Effect of Coloring Pigment on Asphalt Mixture Performance: Case for Use in Ontario, in: Transportation Research Board 95th Annual Meeting, Washington, DC, 2016.Google Scholar
  37. [37]
    J.-P. Planche, Insights into binder chemistry, microstructure, properties relationships & usage in the real world, in: ISAP 2014, CRC Press, Raleigh, USA, 2014, pp. 13–20.Google Scholar
  38. [38]
    H. Collins-Garcia, T. Mang, R. Roque, B. Choubane, An evaluation of an alternative solvent for extraction of asphalt to reduce health and environmental hazards, in: 79th Annual Meeting of the Transportation Research Board, Washington, DC, 2000.Google Scholar
  39. [39]
    H.U. Bahia, D. Swiertz, Design System for HMA Containing a High Percentage of RAS Material, University of Wisconsin, Madison, Wisconsin, 2011.Google Scholar
  40. [40]
    N. Piérard, A. Vanelstraete, Extraction et récupération des bitumes modifiés aux polymères (SBS, EVA) contenus dans les enrobés bitumineux sur base des normes d’essai EN 12697-1 et -3 [Extraction and recovery of polymer modified bitumen (SBS, EVA) from asphalt mixtures on the basis of EN 12697-1&3], in: Congrès Belge de La Route, Ghent, Belgium, 2009.Google Scholar
  41. [41]
    L.E. Tibbits, Implementation of the Vacuum Extraction Method for the Determination of Asphalt Binder Content, Michigan Department of Transportation, 2005.Google Scholar
  42. [42]
    American Association of State Highway and Transportation Officials, Standard Test Method for the Quantitative Extraction and Recovery of Asphalt Binder from Asphalt Mixtures. AASHTO TP2. Washington DC, USA, 2001.Google Scholar
  43. [43]
    American Association of State Highway and Transportation Officials, Standard Method of Test for Quantitative Extraction and Recovery of Asphalt Binder from Asphalt Mixtures. AASHTO T 319. Washington DC, USA, 2015.Google Scholar
  44. [44]
    American Society for Testing and Materials, Standard Test Method for Quantitative Extraction and Recovery of Asphalt Binder from Asphalt Mixtures. ASTM D 6847. West Conshohocken, PA, USA, 2002.Google Scholar
  45. [45]
    M. Anderson, Introduction to Asphalt Extraction/Recovery Procedures, in: Recovery Procedures and Testing of Recovered Asphalt Binders Seminar Hosted by the Technical Advisory Committee, Montreal, Quebec, 2017.Google Scholar
  46. [46]
    R.S. McDaniel, H. Soleymani, R.M. Anderson, P. Turner, R. Peterson, Recommended use of reclaimed asphalt pavement in the Superpave mix design method. Web Document 30 (Project D9-12). National Cooperative Highway Research Program, Lexington, Kentucky, USA, 2000.Google Scholar
  47. [47]
    M.J. Farrar, R.W. Grimes, S. Wiseman, J.-P. Planche, Asphalt Pavement–Micro-sampling and Micro-extraction Methods. FHWA Contract No. DTFH61-07-D-00005. Western Research Institute, 2015.Google Scholar
  48. [48]
    S. Glidden, Automated Extraction of Asphalt Binder, in: Asphalt Binder Expert Task Group, Ames, Iowa, 2017.Google Scholar
  49. [49]
    M. Heitzman, Design and construction of asphalt paving materials with crumb rubber modifier, Transp. Res. Rec. 1339 (1992).Google Scholar
  50. [50]
    G. Abson, Method and Apparatus for the Recovery of Asphalt, in: ASTM Proceedings, 1933, pp. 704–714.Google Scholar
  51. [51]
    H. Collins-Garcia, M. Tia, R. Roque, B. Choubane, Alternative solvent for reducing health and environmental hazards in extracting asphalt: An evaluation, Transp. Res. Rec. 1712(1) (2000) 79–85.Google Scholar
  52. [52]
    B.L. Burr, R.R. Davison, C.J. Glover, J.A. Bullin, Solvent Removal from Asphalt, Transp. Res. Rec. 1269 (1990) 1–8.Google Scholar
  53. [53]
    Ministry of Transportation Ontario, Ontario Test Method, Method of test for recovery of asphalt from solution by Abson or Rotavapor. LS 284. ON, USA, 1996.Google Scholar
  54. [54]
    American Society for Testing and Materials, Standard Practice for Recovery of Asphalt from Solution Using the Rotary Evaporator. ASTM D 5404. West Conshohocken, PA, USA, 2012.Google Scholar
  55. [55]
    European Committee for Standardization (CEN), Bituminous mixtures. Test methods. Bitumen recovery: Rotary evaporator. EN 12697-3. Brussels, Belgium, 2013.Google Scholar
  56. [56]
    J. McGraw, E. Johnson, G. Johnson, S. Dai, D. Linell, M. Watson, Incorporation of recycled asphalt shingles in hot-mixed asphalt pavement mixtures. No. MN/RC 2010-08. Minnesota Department of Transportation, Minnesota, USA, 2010.Google Scholar
  57. [57]
    T. Houser, Bitumen extraction from asphalt pavements, U.S. Patent No. 5053118 A, Washington DC, 1991.Google Scholar
  58. [58]
    R.E. Doherty, A History of the Production and Use of Carbon Tetrachloride, Tetrachloroethylene, Trichloroethylene and 1,1,1-Trichloroethane in the United States: Part 2–Trichloroethylene and 1,1,1-Trichloroethane, Environ. Forensics 1 (2000) 83–93.Google Scholar
  59. [59]
    P. Mikhailenko, G. Webber, H. Baaj, Evaluation of solvents for asphalt extraction, Road Mater. Pave. Des. (2019) https://doi.org/10.1080/14680629.2019.1661277.Google Scholar
  60. [60]
    UN Ozone Secretariat, The Montreal protocol on substances that deplete the ozone layer, in: United Nations Environment Programme, Nairobi, Kenya, 2000.Google Scholar
  61. [61]
    L. Ziyani, L. Boulangé, A. Nicolaï, V. Mouillet, Bitumen extraction and recovery in road industry: A global methodology in solvent substitution from a comprehensive review, J. Clean. Production 161 (2017) 53–68.Google Scholar
  62. [62]
    J. McGraw, D. Iverson, G. Schmidt, J. Olson, Selection of an alternative asphalt extraction solvent. No. MN/RC-2003-35. Minnesota Department of Transportation, Minnesota, USA, 2001.Google Scholar
  63. [63]
  64. [64]
    Federal-Provincial Advisory Committee on Environmental and Occupational Health (Canada), ed., Exposure guidelines for residential indoor air quality: a report of the Federal-Provincial Advisory Committee on Environmental and Occupational Health, Rev, Health and Welfare Canada, Ottawa, Ont, 1989.Google Scholar
  65. [65]
  66. [66]
    Toxicological Profile for Trichloroethylene (TCE), (Agency for Toxic Substances and Disease Registry, 2015) https://www.atsdr.cdc.gov/ToxProfiles/tp19.pdf.Google Scholar
  67. [67]
    Ministry of Transportation, Ontario Test Method, Method of test for quantitative extraction of asphalt cement and analysis of extracted aggregate from bituminous paving mixtures. LS 282. ON, USA, 2010.Google Scholar
  68. [68]
    Z. Hossain, P. Solanki, M. Zaman, D. Adje, S. Lewis, Test Methods For Use of Recycled Asphalt Pavement in Asphalt Mixes, College of Engineering. Vol. 107. FHWA-OK-12-01. University of Oklahoma, OK, USA, 2012.Google Scholar
  69. [69]
    L. Clark, EnSolv Vapor Degreasing and Cleaning Solvent, EnviroTech International, Melrose Park, III, 1998.Google Scholar
  70. [70]
    I. Urbina, As OSHA Emphasizes Safety, Long-Term Health Risks Fester, The New York Times, 2013.Google Scholar
  71. [71]
    National Toxicology Program, 13th Report on carcinogens, US Department of Health and Human Services, Research Triangle Park, NC, 2014.Google Scholar
  72. [72]
    S.-W. Loh, J. Olek, Contributions of PG graded asphalt to low temperature cracking resistance of pavement, Purdue University Department of Civil Engineering, 1999 https://doi.org/10.5703/1288284313168.Google Scholar
  73. [73]
    American Society for Testing and Materials, Standard Practice for Recovery of Asphalt from Solution Using Toluene and the Rotary Evaporator. ASTM D 7906. West Conshohocken, PA, USA, 2012.Google Scholar
  74. [74]
    B. Va, Health effects of toluene: a review, Neurotoxicology 2 (1981) 567–588.Google Scholar
  75. [75]
    A.K. Low, J.R. Meeks, C.R. Mackerer, Health Effects of the Alkylbenzenes. I. Toluene, Toxicology and Industrial Health 4 (1988) 49–75.Google Scholar
  76. [76]
    M. Glor, A Synopsis of Explosion Hazards During the Transfer of Powders into Flammable Solvents and Explosion Preventative Measures, Pharmaceutical Eng. 30 (1) (2010) 56.Google Scholar
  77. [77]
    T.S.S. Dikshith, Handbook of Chemicals and Safety, CRC Press, Boca Raton, Florida, USA, 2016.Google Scholar
  78. [78]
    C.A. Cipione, R.R. Davison, B.L. Burr, C.J. Glover, J.A. Bullin, Evaluation of solvents for extraction of residual asphalt from aggregates, Transp. Res. Rec. 1323 (1991) 47–52.Google Scholar
  79. [79]
    Y. Gu, F. Jérôme, Bio-based solvents: an emerging generation of fluids for the design of eco-efficient processes in catalysis and organic chemistry, Chem. Soc. Rev. 42 (2013) 9550–9570.Google Scholar
  80. [80]
    A. Falk Filipsson, J. Bard, S. Karlsson, Limonene, World Health Organization, Geneva, 1998.Google Scholar
  81. [81]
    T. Bennert, Discussion of 2015 ASTM Binder Recovery ILS, in: Recovery Procedures and Testing of Recovered Asphalt Binders Seminar Hosted by the Technical Advisory Committee, Montreal, Quebec, 2017.Google Scholar
  82. [82]
    P. Mikhailenko, Valorisation of by-products and products from agro-industry for the development of release and rejuvenating agents for bituminous materials, (PhD Thesis), Universite Paul Sabatier Toulouse III, Toulouse France, 2015.Google Scholar

Copyright information

© Chinese Society of Pavement Engineering. Production and hosting by Springer Nature 2019

Authors and Affiliations

  • Peter Mikhailenko
    • 1
    • 2
    Email author
  • Parinaz Ataeian
    • 2
  • Hassan Baaj
    • 2
  1. 1.Road Materials and Sealing Components, EmpaSwiss Federal Laboratories for Materials Science and TechnologyDübendorfSwitzerland
  2. 2.Centre for Pavement and Transportation Technology (CPATT), Department of Civil & Environmental EngineeringUniversity of WaterlooWaterlooCanada

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