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Microstructure and magnetic properties of Fe81.3Si4B13Cu1.7 nanocrystalline alloys with minor Nb addition

  • Xiang-cheng Ren
  • Yan-hui Li
  • Xing-jie Jia
  • Zhi-yong Qiu
  • Guo-qiang Xie
  • Wei Zhang
Original Paper
  • 64 Downloads

Abstract

The amorphous matrix containing dispersive high number density (Nd) α-Fe nuclei with average grain sizes (D) of 4.3–6.2 nm was formed in the melt-spun Fe81.3–xSi4B13Cu1.7Nbx (x = 0–2) alloys, and the Nd and D values reduce with increase in the Nb content. The fine nanocrystalline structure with α-Fe grains of 14.0–21.6 nm in size was obtained for the annealed alloys, which showed high saturation magnetic flux density of 1.60–1.77 T and low coercivity (Hc) of 7.1–17.0 A/m. Addition of minor Nb significantly expands the optimum annealing temperature range for obtaining good soft magnetic properties, while coarsens the α-Fe grains, leading to a slight increase in the Hc. The mechanism of the effect of Cu and Nb elements on the structure and magnetic properties was discussed in terms of the formation and growth of the α-Fe nuclei of the alloys.

Keywords

Fe-based nanocrystalline alloy Soft magnetic property Cu content α-Fe nuclei Nb alloying 

Notes

Acknowledgements

This research was supported by the National Key Research and Development Program of China (Grant No. 2017YFB0903903) and the National Natural Science Foundation of China (Grant Nos. 51571047, 51771039).

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Copyright information

© China Iron and Steel Research Institute Group 2018

Authors and Affiliations

  • Xiang-cheng Ren
    • 1
  • Yan-hui Li
    • 1
  • Xing-jie Jia
    • 1
  • Zhi-yong Qiu
    • 1
  • Guo-qiang Xie
    • 2
  • Wei Zhang
    • 1
  1. 1.Key Laboratory of Solidification Control and Digital Preparation Technology (Liaoning Province), School of Materials Science and EngineeringDalian University of TechnologyDalianChina
  2. 2.School of Materials Science and EngineeringHarbin Institute of Technology (Shenzhen)ShenzhenChina

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