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Grown of highly porous ZnO-nanoparticles by pulsed laser ablation in liquid technique for sensing applications

  • Shumaila Islam
  • Hazri Bakhtiar
  • Khaldoon N. Abbas
  • Saira Riaz
  • Shahzad Naseem
  • Abdul Rahman Bin Johari
Research
  • 17 Downloads

Abstract

Pulsed laser ablation technique in deionized water with low laser fluency has been explored to prepare uniform dispersed porous ZnO nanoparticles for sensing applications. Surface morphology, particle size, porous structure, roughness, elemental distribution, and chemical bonding of the synthesized ZnO are analyzed by TEM, FESEM, AFM, EDX, and FTIR spectroscopy, respectively. Sensing behavior is observed by UV–Vis absorption measurements. TEM and FESEM analysis show that the prepared ZnO-coated film has homogeneous, dispersed, highly porous, and crack-free surface; the average particle size are observed ~ 24.72 ± 2.97 nm. The porous structure is responsible for appropriate sensing behavior. Low roughness value ~ 1.52 nm which is analyzed by AFM is advantageous for sensing behavior. EDX spectrum and elements mapping clearly show the uniform Zn and O distribution. XRD analysis confirms the hexagonal wurtzite structure of ZnO. FTIR reveals the Zn and O chemical bonding successfully. UV-Visible analysis exhibits that the prepared ZnO matrix has good incorporation with multi-dyes solutions at pH values 10–12 with significant changes in color behavior. The highest pKa value ~ 9.77 at a wavelength of 598.28 nm was calculated for multi-dyes immobilized ZnO matrix. So, it can be concluded that prepared ZnO nanostructures are potential candidates for sensing application.

Keywords

PLAL technique ZnO nanostructures pH sensing Indicator dyes Crack-free surface 

Notes

Funding information

Shumaila Islam received financial support from the Universiti Teknologi Malaysia, through RMC under the Postdoctoral Fellowship for the performance and management of the project. Corresponding author is supported by the Malaysian Ministry of Education through the FRGS fund with vote 03E89.

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Copyright information

© Australian Ceramic Society 2018

Authors and Affiliations

  • Shumaila Islam
    • 1
  • Hazri Bakhtiar
    • 1
  • Khaldoon N. Abbas
    • 2
  • Saira Riaz
    • 3
  • Shahzad Naseem
    • 3
  • Abdul Rahman Bin Johari
    • 1
  1. 1.Laser Centre, Ibnu Sina Institute for Scientific and Industrial ResearchUniversiti Teknologi MalaysiaSkudaiMalaysia
  2. 2.Faculty of Science, Physics DepartmentAl-Mustansiriya UniversityBaghdadIraq
  3. 3.Centre of Excellence in Solid State PhysicsUniversity of the PunjabLahorePakistan

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