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Nanosize Metal Schiff Base Complexes as Precursors for the Preparation of HgO, Co3O4 and Mn3O4 Nanoparticles

  • Aliakbar Dehno KhalajiEmail author
  • Shaghayegh Izadi
  • Gholamhossein Grivani
Research Paper
  • 18 Downloads

Abstract

In this paper, nanosize metal Schiff base complexes M((nac)2en)Cl2, (nac)2en = N,N′-bis(paranitroacetophenone)ethylenediamine, M = Hg (1), Co (2) and Mn (3), have been prepared by ultrasonic bath assisted and were characterized by elemental analyses (CHN) and SEM. The thermal behavior of the complexes from room temperature to 700 °C shows different weight losses. In addition, the complexes used as new precursors for preparation of metal oxide nanoparticles by solid-state thermal decomposition at 600 °C. Metal oxide nanoparticles were characterized by FT-IR, XRD and SEM.

Keywords

Nanosize complexes Mercury(II) Cobalt(II) Manganese(II) Metal oxides 

Notes

Acknowledgements

The financial support from the Golestan University and Damghan University are gratefully acknowledged.

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Copyright information

© Shiraz University 2017

Authors and Affiliations

  • Aliakbar Dehno Khalaji
    • 1
    Email author
  • Shaghayegh Izadi
    • 1
  • Gholamhossein Grivani
    • 2
  1. 1.Department of Chemistry, Faculty of ScienceGolestan UniversityGorganIran
  2. 2.School of ChemistryDamghan UniversityDamghanIran

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