Acta Metallurgica Sinica (English Letters)

, Volume 31, Issue 2, pp 189–198 | Cite as

Effect of Solution Treatment on the Microstructure and Mechanical Properties of Sand-Cast Mg–9Gd–4Y–0.5Zr Alloy

  • Jing-Li Li
  • Na Zhang
  • Xiao-Xuan Wang
  • Di WuEmail author
  • Rong-Shi ChenEmail author


Sand-cast Mg–9Gd–4Y–0.5Zr (wt%) alloy was solution-treated at 500–565 °C in the time range of 0.5–30 h in air or vacuum to investigate its microstructure evolution and mechanical properties. The results showed that solution treatment temperature had a significant influence on the dissolving rate of eutectic phase and grain growth. Taken both of them into consideration, 510–520 °C was considered to be the optimum solution treatment temperature range for this alloy. It should be noted that the trace (0.4–0.9 vol%) and insoluble cuboid-shaped phase precipitated during solution treatment was identified to be YH2, of which the hydrogen was thought to come from both the melting and solution heating process. In addition, the 3D morphology and dissolving process of Mg24(Gd,Y)5 eutectic phases in the as-cast alloy were also discussed via in-situ observation under X-ray tomography.


Mg–Gd–Y–Zr alloy Solution treatment Microstructure Rare-earth hydride 



This work was funded by the National Natural Science Foundation of China (Grant Nos. 51301173 and 51531002), the National Basic Research Program of China (973 Program) (Grant No. 2013CB632202), and the National Key Research and Development Program of China (Grant No. 2016YFB0301104).


  1. [1]
    Z. Yang, J. Li, J. Zhang, G. Lorimer, J. Robson, Acta Metall. Sin. (Engl. Lett.) 21, 313 (2008)CrossRefGoogle Scholar
  2. [2]
    Y. Liu, G. Yuan, C. Lu, W. Ding, J. Jiang, J. Mater. Sci. 43, 5527 (2008)CrossRefGoogle Scholar
  3. [3]
    R.B. Figueiredo, T.G. Langdon, J. Mater. Sci. 43, 7366 (2008)CrossRefGoogle Scholar
  4. [4]
    S. Zhang, S. Chen, Y. Ma, H. Song, M. Cheng, Acta Metall. Sin. (Engl. Lett.) 28, 1452 (2015)CrossRefGoogle Scholar
  5. [5]
    L. Gao, R.S. Chen, E.H. Han, J. Mater. Sci. 44(4443), 4443 (2009)CrossRefGoogle Scholar
  6. [6]
    Y. Guo, J. Li, J. Li, Z. Yang, J. Zhao, F. Xia, M. Liang, J. Alloys Compd. 450, 446 (2008)CrossRefGoogle Scholar
  7. [7]
    S. He, X.Q. Zeng, L. Peng, X. Gao, J. Nie, W. Ding, J. Alloys Compd. 427, 316 (2007)CrossRefGoogle Scholar
  8. [8]
    I.A. Anyanwu, S. Kamado, Y. Kojima, Mater. Trans. 42, 1206 (2001)CrossRefGoogle Scholar
  9. [9]
    S. He, X.Q. Zeng, L. Peng, X.Q. Gao, J. Nie, W. Ding, J. Alloys Compd. 421, 309 (2006)CrossRefGoogle Scholar
  10. [10]
    Y. Gao, Q. Wang, J. Gu, Y. Zhao, Y. Tong, Mater. Sci. Eng., A 459, 117 (2007)CrossRefGoogle Scholar
  11. [11]
    S. Zhu, J. Nie, M. Gibson, M. Easton, Scr. Mater. 77, 21 (2014)CrossRefGoogle Scholar
  12. [12]
    W. Zheng, X. Li, K. Zhang, M. Ma, Y. Li, G. Shi, J. Yuan, Chin. J. Nonferr. Metal. 25(5), 1136 (2015)Google Scholar
  13. [13]
    G. Lin, Z. Zhang, H. Zhang, D. Peng, J. Zhou, Acta Metall. Sin. (Engl. Lett.) 21, 109 (2008)CrossRefGoogle Scholar
  14. [14]
    R. Hamilton, M. Forster, R. Dashwood, P. Lee, Scr. Mater. 46, 25 (2002)CrossRefGoogle Scholar
  15. [15]
    H. Nodooshan, G. Wu, W. Liu, G. Wei, Y. Li, S. Zhang, Mater. Sci. Eng., A 651, 840 (2016)CrossRefGoogle Scholar
  16. [16]
    L. Gao, J. Zhou, Z. Sun, R. Chen, E. Han, Chin. Sci. Bull. 56, 1038 (2011)CrossRefGoogle Scholar
  17. [17]
    Q. Peng, Y. Huang, J. Meng, Y. Li, K.U. Kainer, Intermetallics 19, 382 (2011)CrossRefGoogle Scholar
  18. [18]
    K. Zheng, J. Dong, X. Zeng, W. Ding, Mater. Sci. Technol. 24, 320 (2008)CrossRefGoogle Scholar
  19. [19]
    Z. Mu, Dissertation, Central South University, 2013Google Scholar
  20. [20]
    K. Lu, L. Lu, S. Suresh, Science 324, 349 (2009)CrossRefGoogle Scholar
  21. [21]
    L. Gao, R. Chen, E. Han, J. Alloys Compd. 481, 379 (2009)CrossRefGoogle Scholar
  22. [22]
    Y. Xu, D. Xu, X. Shao, E. Han, Acta Metall. Sin. (Engl. Lett.) 26, 217 (2013)CrossRefGoogle Scholar

Copyright information

© The Chinese Society for Metals and Springer-Verlag Berlin Heidelberg 2017

Authors and Affiliations

  1. 1.The Group of Magnesium Alloys and Their ApplicationsInstitute of Metal Research, Chinese Academy of SciencesShenyangChina
  2. 2.School of Materials Science and EngineeringUniversity of Science and Technology of ChinaHefeiChina
  3. 3.AVIC Shenyang Liming Aero—Engine Group CorporationShenyangChina

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