Mechanical Properties of Steam Cured High-Strength Steel Fiber-Reinforced Concrete with High-Volume Blast Furnace Slag
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Abstract
In this study, the effects of water-to-binder (W/B) ratio and replacement ratio of blast furnace slag (BFS) on the compressive strength of concrete were first investigated to determine an optimized mixture. Then, using the optimized high-strength concrete (HSC) mixture, hooked steel fibers with various aspect ratios and volume fractions were used as additives and the resulting mechanical properties under compression and flexure were evaluated. Test results indicated that replacement ratios of BFS from 50 to 60% were optimal in maximizing the compressive strength of steam-cured HSCs with various W/B ratios. The use of hooked steel fibers with the aspect ratio of 80 led to better mechanical performance under both compression and flexure than those with the aspect ratio of 65. By increasing the fiber aspect ratio from 65 to 80, the hooked steel fiber volume content could be reduced by 0.25% without any significant deterioration of energy absorption capacity. Lastly, complete material models of steel-fiber-reinforced HSCs were proposed for structural design from Lee’s model and the RILEM TC 162-TDF recommendations.
Keywords
high-strength concrete blast furnace slag hooked steel fiber aspect ratio mechanical property material model1 Introduction
In recent years, the development of green concrete with low CO2 emissions has received a great deal of attention from researchers worldwide (Bilodeau and Malhotra 2000; Menéndez et al. 2003; Mahmoud et al. 2013; Kinoshita et al. 2014). The production of Portland cement contributes a large portion of anthropogenic CO2 emissions; thus, a key challenge is to reduce the amount of cement used in concrete mixtures. Replacing Portland cement with mineral admixtures such as fly ash, blast furnace slag (BFS), and silica fume has been a widely adopted strategy due to their pozzolanic reactivity and latent hydraulic activity (Jeon et al. 2006; Roychand et al. 2016). In particular, if the size of mineral particles is properly determined, then they can be used to fabricate concrete mixtures stronger than those without mineral admixtures. High-strength concrete (HSC) has many advantages for use in precast pre- or post-tensioned structures, which are normally steam-cured with heat. Thus, optimized mixtures need to be developed for steam-cured HSCs incorporating high volumes of mineral admixtures.
HSC is intrinsically brittle, exhibiting low fracture energy. This has limited the practical applications of HSC in real civil and architectural structures, and is especially limiting for designs subjected to tension or flexure. Several methods have been used to improve the ductility and energy absorption capacity of concrete, such as adding discontinuous fibers (i.e. steel, polymeric, and carbon fibers) and strengthening with fiber-reinforced polymers (Banthia and Nandakumar 2006; Myers et al. 2008; Kwon et al. 2015; Yoo and Yoon 2016d). The use of discontinuous fibers has been the most widely adopted method because it is the simplest and most effective in improving the ductility of concrete. According to a previous study performed by Bindiganavile and Banthia (2001), the use of steel fibers improved static post-cracking flexural behavior relative to polymeric fibers, especially at small deflections, because the polymeric fibers allowed wider cracks to form that carry tensile stress further beyond the matrix cracking. Yao et al. (2003) also reported much better flexural performance in concretes using steel fibers compared to those using polymeric fibers. Soroushian and Bayasi (1991) experimentally investigated the effect of steel fiber shape on the mechanical properties of concrete, and found that the use of hooked steel fibers having various aspect ratios was more effective in improving the flexural strength, energy absorption capacity, and post-peak ductility under compression than the use of straight and crimped fibers at identical volume fractions of 2%. Thus, among the various types of steel and polymeric fibers available, synthetically hooked steel fibers are expected to be most efficient in improving the flexural performance of concrete under static loads assuming identical amount of added fibers.
To allow the practical use of such fiber-reinforced concrete (FRC) in actual structures, its material models need to be preferentially proposed. Fibers incorporated into the cement matrix inhibit crack propagation and widening, leading to different post-cracking behaviors under compression and tension compared to those of ordinary concrete without fiber. For this reason, several researchers (Barros et al. 2005) have previously used RILEM TC 162-TDF recommendations (RILEM 2000), one of the most widely used model codes for FRC compositions including metallic fibers. However, RILEM TC 162-TDF recommends the use of a compressive model of FRC that is identical to that used for ordinary concrete, even though FRC’s post-peak ductility is substantially influenced by the fibers (Yoo et al. 2015). Thus, it is reasonable to develop a model of tensile stress and strain (TSS) based on RILEM TC 162-TDF and to develop a better model of compressive stress and strain (CSS) based instead upon previously suggested compressive models for FRC.
Accordingly, in the present study, the effects of water-to-binder (W/B) ratio and BFS replacement ratio upon concrete compressive strength were first examined to determine optimized mix proportions. Then, the mechanical properties of the optimized HSC were investigated for various aspect ratios and volume fractions of hooked steel fiber additive. Based upon our work, herein we propose complete material models of steel-fiber-reinforced HSC (SFR-HSC) based on previous models and the RILEM TC 162-TDF recommendations.
2 Test Program
2.1 Materials, Mixture Proportions, and Curing Condition
Mixture proportions.
W/B (%) | BFS/B (%) | s/a (%) | Unit weight (kg/m3) | |||||
---|---|---|---|---|---|---|---|---|
Water | Cement | BFS | Fine aggregate | Coarse aggregate | AEWR agent | |||
25.0 | 0 | 43.7 | 163 | 652 | 0 | 682 | 882 | 0.80 |
40 | 42.0 | 391 | 261 | 647 | 897 | 0.65 | ||
50 | 41.7 | 326 | 326 | 641 | 899 | 0.70 | ||
60 | 41.4 | 261 | 391 | 634 | 901 | 0.75 | ||
70 | 41.1 | 196 | 456 | 628 | 903 | 0.70 | ||
27.5 | 0 | 43.7 | 593 | 0 | 703 | 909 | 0.77 | |
40 | 43.0 | 356 | 237 | 685 | 911 | 0.60 | ||
50 | 42.7 | 296 | 296 | 678 | 913 | 0.63 | ||
60 | 42.4 | 237 | 356 | 671 | 916 | 0.70 | ||
70 | 42.1 | 178 | 415 | 665 | 918 | 0.68 | ||
30.0 | 0 | 43.7 | 543 | 0 | 721 | 932 | 0.80 | |
40 | 44.0 | 326 | 217 | 719 | 919 | 0.63 | ||
50 | 43.7 | 272 | 272 | 712 | 921 | 0.60 | ||
60 | 43.4 | 217 | 326 | 706 | 924 | 0.68 | ||
70 | 43.1 | 163 | 380 | 699 | 927 | 0.70 |
Chemical compositions and physical properties of Type I Portland cement.
Surface area (cm2/g) | Density (g/cm3) | Ig.loss (%) | Chemical composition (%) | |||||
---|---|---|---|---|---|---|---|---|
SiO2 | Al2O3 | Fe2O3 | CaO | MgO | SO3 | |||
3413 | 3.15 | 1.40 | 21.25 | 5.28 | 3.02 | 61.00 | 3.71 | 1.24 |
Chemical compositions and physical properties of Type III blast furnace slag.
Surface area (cm2/g) | Density (g/cm3) | Ig.loss (%) | Chemical composition (%) | ||
---|---|---|---|---|---|
SiO2 | MgO | Cl− | |||
4250 | 2.90 | 0.32 | 21.01 | 6.40 | 0.005 |
Properties of hooked steel fibers.
Name | Diameter, d f (mm) | Length, l f (mm) | Aspect ratio (l f /d f ) | Density (g/cm3) | Tensile strength (MPa) | Elastic modulus (GPa) |
---|---|---|---|---|---|---|
Short HS | 0.55 | 35 | 65 | 7.9 | 1400 | 200 |
Long HS | 0.75 | 60 | 80 | 7.9 | 1100 | 200 |
Temperature history for steam curing.
2.2 Test Setup and Specimen Preparation
2.2.1 Compression
Compressive test (ASTM C39).
2.2.2 Four-Point Flexure
Four-point flexural test (ASTM C1609).
2.2.3 Three-Point Flexure for Notched Beams
Three-point flexural test for notched beam (RILEM TC 162-TDF).
3 Test Results and Discussion
3.1 Effects of W/B and Replacement Ratio of BFS on Compressive Strength
Summary of compressive strength; a W/B of 0.3, b W/B of 0.275, c W/B of 0.25.
Effect of replacement ratio of BFS on compressive strength; a W/B of 0.3, b W/B of 0.275, c W/B of 0.25.
The chief aim of the present study was to develop low-carbon HSC mixtures for precast prestressed products; thus the initial strength immediately after heat curing was the most important parameter. The highest 1-d compressive strength of 56.7 MPa was obtained from mixture BS60 at the W/B of 0.275. In addition, when a W/B ratio of 0.25 was used, the workability was obviously deteriorated and slightly higher AE agent was required, as compared with W/B ratio of 0.275 or 0.3. Thus, this mixture was considered optimal for precast prestressed concrete products in this study.
3.2 Properties of SFR-HSC
ACI Subcommittee 318-F recommended the use of a minimum fiber volume fraction (V f ) of 0.75% for replacing minimum shear reinforcement through the use of steel fibers (Parra-Montesinos 2006). Thus, we first used the V f of 0.75 vol.% of hooked steel fibers having the aspect ratio of 65. According to previous studies (Yazıcı et al. 2007; Yoo and Yoon 2015; Yoo et al. 2016b), the use of steel fibers having higher aspect ratios exhibited better flexural performance than those having lower aspect ratios. Thus, to investigate whether the content of hooked steel fibers could be reduced by increasing the aspect ratio, concrete beams including 0.5 vol.% of hooked steel fibers with the higher aspect ratio of 80 were also prepared and tested. Also, to fundamentally evaluate how much the flexural performance of HSC beams could be improved by increasing the fiber aspect ratio, a specimen containing 0.5 vol.% of hooked steel fibers having the smaller aspect ratio of 65 was also prepared and tested. The optimized mixture (BS60 with W/B of 0.275) was used, and thus the designation system adopted herein for such samples only specifies the fiber aspect ratio and volume fraction, as follows: aspect ratio of steel fiber (Sxx)-volume fraction (0. yy). Herein, xx and yy respectively represent the aspect ratio and volume fraction. For example, S65-0.75 indicates the specimen including 0.75 vol.% of steel fibers each having the aspect ratio of 65.
3.2.1 Compressive Behaviors
Average compressive stress versus strain curves (after 28 days).
Summary of compressive properties (at 28 days).
Name | Compressive strength (MPa) | Strain capacity (mm/mm) | Elastic modulus (GPa) |
---|---|---|---|
OPC | 67.0 | 0.00310 | 32.0 |
S65-0.5 | 70.3 | 0.00320 | 33.0 |
S80-0.5 | 72.0 | 0.00326 | 32.9 |
S65-0.75 | 67.9 | 0.00292 | 33.0 |
To predict the compressive behaviors of SFR-HSC, the following equation suggested by Lee et al. (2015) was adopted.
In Fig. 7, the dotted line indicates the values predicted by Eq. (1). An empirical equation proposed by Lee et al. (2015) appeared to be appropriate for predicting the compressive behavior of SFR-HSC with high-volume BFS, for both ascending and descending branches.
3.2.2 Flexural Behaviors
Flexural load versus deflection curves (four-point flexure).
Parameters obtained from four-point flexural tests (ASTM C1609).
Name | F LOP (MPa) | F MOR (MPa) | δ MOR (mm) | Tough L/600 (kNmm) | Tough L/150 (kNmm) | F R,L/300 (MPa) | F R,L/150 (MPa) |
---|---|---|---|---|---|---|---|
OPC | 7.0 | 7.0 | 0.063 | – | – | – | – |
S65-0.5 | 7.8 | 8.0 | 0.85 | 10.8 | 48.4 | 8.0 (103%) | 6.8 (87%) |
S80-0.5 | 7.2 | 9.8 | 1.72 | 12.5 | 59.8 | 9.4 (131%) | 9.6 (133%) |
S65-0.75 | 9.2 | 10.0 | 0.87 | 14.1 | 60.9 | 9.9 (108%) | 8.3 (90%) |
The toughness values at two deflection points of L/600 and L/150 were calculated according to ASTM C1609 (ASTM 2012); L is the clear span length. Because the specimen without fibers exhibited a sudden load drop immediately after the first cracking (at 0.063 mm deflection), its toughness was not calculated. Specimen S65-0.75 exhibited the highest toughnesses at both deflection points because it had the largest amount of steel fibers among the specimens studied. However, specimen S80-0.5 demonstrated toughness values quite similar to those of S65-0.75 despite its lower amount of fibers, and showed higher toughness values than S65-0.5. This indicates that the use of steel fibers with higher aspect ratios can reduce the amount of fibers needed without any noticeable reduction of energy absorption capacity, a finding consistent with previous findings mentioned above regarding flexural strength and deflection capacity.
ACI 318-14 code (ACI 2014) indicates that concrete with steel fibers can be used for shear resistance provided that the residual strengths, f R, obtained from four-point flexural tests (ASTM C1609) at the deflection points of L/300 and L/150 are greater than 90 and 75% of the f LOP. Therefore, the residual flexural stress was also investigated; Table 6 summarizes the results. All test series satisfied the requirements of the ACI 318 code. This means that SFRC containing 0.5 vol.% of hooked steel fibers having aspect ratios higher than 65 are suitable to be used to impart shear resistance. Interestingly, the residual flexural strengths were increased more significantly with increasing fiber aspect ratio than with a small increase in the amount of steel fibers. Thus, it was concluded that using steel fibers with higher aspect ratios is effective in increasing residual strength, affecting shear resistance, than using those with smaller ones.
3.2.3 Suggestion of Tensile Stress Block for Structural Design
Flexural load versus deflection curves (three-point flexure).
The flexural strengths at the points of LOP and MOR obtained in the larger beams were clearly lower than those obtained in the smaller beams (in Fig. 8). This was mainly caused by the size effect and restraint of the support. Decreases in the strength of normal- and high-strength SFRC beams has been previously reported by Yoo et al. (2016c). In accordance with Weibull’s size effect theory (Weibull 1939), larger specimens are normally weaker than smaller ones because they have a greater chance to include larger and more severe flaws. The three-point flexural tests were performed using a roller-type support to eliminate the support restraint as per RILEM TC 162-TDF, whereas the four-point flexural tests were carried out using a pin-type support as per ASTM C1609. In test results reported by Wille and Parra-Montesinos, the measured flexural strength was clearly affected by the support conditions: use of the pin-type support resulted in a higher flexural strength than the roller-type support due to its restraint by friction (Wille and Parra-Montesinos 2012).
To calculate a tensile stress block, RILEM TC 162-TDF recommendations were adopted in this study. Firstly, equivalent flexural strengths were calculated based on energy absorption capacities, as follows:
Parameters for modeling tensile stress block of SFR-HSC.
Name | \( D_{BZ,2}^{f} \) (kNmm) | \( D_{BZ,3}^{f} \) (kNmm) | F eq,2 (MPa) | F eq,3 (MPa) | σ 1 (MPa) | σ 2 (MPa) | σ 3 (MPa) | ε 1 (mm/mm) | ε 2 (mm/mm) | ε 3 (mm/mm) |
---|---|---|---|---|---|---|---|---|---|---|
S65-0.5 | 7.7 | 37.1 | 4.93 | 4.75 | 6.92 | 2.22 | 1.76 | 0.00021 | 0.00031 | 0.025 |
S80-0.5 | 10.7 | 56.3 | 6.85 | 7.21 | 7.80 | 3.08 | 2.79 | 0.00024 | 0.00034 | 0.025 |
S65-0.75 | 14.3 | 55.1 | 9.15 | 7.05 | 8.20 | 4.12 | 2.61 | 0.00025 | 0.00035 | 0.025 |
Material modeling.
Here, f MOR is the flexural strength, d is the effective beam depth, and E c is the elastic modulus of concrete.
Tensile stress versus strain models.
Complete material models under compression and tension for the SFR-HSC used in the current study were obtained by using Lee’s compressive model (Lee et al. 2015) in Eq. (1) and the tensile models, suggested by RILEM TC 162-TDF, with suggested parameters from Table 7. Thus, these models can be adopted for sectional analysis of structural elements made of SFR-HSC.
3.2.4 Fracture Energy
Fracture energy versus COD curves.
4 Conclusions
- 1.
Concrete mixtures with a lower W/B ratio and higher replacement ratios of BFS up to 60% exhibited higher compressive strength than their counterparts. The optimum BFS replacement ratio varied between 50 and 60% in terms of the compressive strength developed in steam-cured HSC both early and during long-term aging.
- 2.
The addition of hooked steel fibers slightly increased the compressive strength and increased the post-peak ductility significantly. In addition, the use of hooked steel fibers with smaller aspect ratios resulted in better HSC compressive behavior. The overall compressive stress–strain curve was predicted well by Lee’s model.
- 3.
HSC beams having V f of 0.5% or more exhibited deflection-hardening behavior. The use of hooked steel fibers with the highest aspect ratio tested of 80 was more effective in improving the flexural strength, deflection capacity, energy absorption capacity, and residual strength affecting shear resistance, relative to the use of hooked steel fibers with a smaller aspect ratio of 65. In particular, increasing the aspect ratio from 65 to 80 allowed a 0.25% volume reduction of the steel fiber content without any noticeable deterioration of energy absorption capacity. Finally, we proposed TSS models with appropriate parameters for all SFR-HSCs tested, based on the RILEM TC 162-TDF recommendations.
- 4.
Fracture energy capacity of SFR-HSC was improved by increasing the aspect ratio or the amount of hooked steel fibers.
Notes
Acknowledgements
This work was supported by the Industrial Strategic Technology Development Program (10063488, Development of Earthquake Resisting Reinforced Concrete using Grade 700 MPa Reinforcing Bars for Enhancement of Seismic Safety) funded By the Ministry of Trade, Industry & Energy (MI, Korea).
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