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Magnetic solid-phase extraction of quercetin on magnetic-activated carbon cloth (MACC)

  • Muhammad Balal Arain
  • Erkan Yilmaz
  • Numan Hoda
  • Tasneem Gul Kazi
  • Mustafa SoylakEmail author
Original Paper
  • 23 Downloads

Abstract

Magnetic-activated carbon cloth (MACC) was synthesized, characterized, and used as magnetic adsorbent in magnetic solid-phase extraction of quercetin prior to UV–visible spectrophotometric determination. Different parameters such as pH, amount of MACC, effect of volume, and elution time were optimized for the determination of quercetin using UV–visible spectrophotometer at 370 nm. In this procedure, quercetin molecules in aqueous sample phase were adsorbed on the 10 mg of the adsorbent at pH 4.0 and desorbed with acidic methanol solution by using vortex mixer. Limit of detection (LOD), limit of quantification (LOQ), and relative standard deviation were found as 1.4 ng mL−1, 4.8 ng mL−1 and lower than 10%, respectively. The applicability of the developed magnetic solid-phase extraction method was proved on onion samples.

Keywords

Quercetin Magnetic solid-phase extraction Activated carbon cloth Spectrophotometry 

Notes

Acknowledgements

Muhammad Balal Arain is very much thankful to the Scientific and Technological Research Council of Turkey (TUBITAK) under “2216 Research Fellowship Programme for Foreign Citizens” for financial support. The authors also would like to thank to Erciyes University, Kayseri, Turkey, for providing all laboratory facilities and pleasant environment.

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Copyright information

© Iranian Chemical Society 2019

Authors and Affiliations

  • Muhammad Balal Arain
    • 1
    • 2
    • 3
  • Erkan Yilmaz
    • 4
    • 5
  • Numan Hoda
    • 6
  • Tasneem Gul Kazi
    • 7
  • Mustafa Soylak
    • 1
    Email author
  1. 1.Department of Chemistry, Faculty of SciencesErciyes UniversityKayseriTurkey
  2. 2.Department of ChemistryUniversity of KarachiKarachiPakistan
  3. 3.Department of ChemistryAbdul Wali Khan UniversityMardanPakistan
  4. 4.Department of Analytical Chemistry, Faculty of PharmacyErciyes UniversityKayseriTurkey
  5. 5.Nanotechnology Research Center (ERNAM)Erciyes UniversityKayseriTurkey
  6. 6.Engineering FacultyAkdeniz UniversityAntalyaTurkey
  7. 7.National Center of Excellence in Analytical ChemistryUniversity of SindhJamshoroPakistan

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