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Modeling and optimization of characterization of nanostructure anodized aluminium oxide membranes

  • Hamed AzamiEmail author
  • Mohammad Reza Omidkhah
Original Paper
  • 9 Downloads

Abstract

This study indicates the importance of statistical analysis and modeling to investigate the synthesis and optimization of anodized aluminium oxide (AAO) properties for template-assisted synthesis of nanostructure particles. The response surface methodology was used to optimize pore size and porosity of AAO. The impacts of four main parameters including type of acidic electrolyte, concentration of acid, bath temperature and electrical potential of anodization on characterization of AAO were investigated. Statistical analysis showed that the linear and quadratic terms of these variables had significant effects. Based on the statistical analysis, a possible mechanism of the anodization was proposed. The proposed mechanism helped us to develop an analytical model. The analytical model could predict the experimental results with an appropriate accuracy. Results indicated the rate-limiting reaction in anodization process is water dissociation which was conducted at the pore bottom of the AAO. In addition, concentrated electrical field at pore base induced water splitting so that the activation energy of water dissociation decreased ten times and reached to \(9898.5~\frac{{\text{J}}}{{{\text{mol}}}}\).

Graphical abstract

Keywords

Anodized aluminium oxide Nanoporous materials Electrochemical synthesis Pore perforation Statistical analysis 

Notes

Acknowledgements

This study was supported by Iranian National Science Foundation (INSF) (Grant no: 92000914). The authors gratefully acknowledge this support.

Supplementary material

13738_2018_1574_MOESM1_ESM.pdf (317 kb)
Supplementary material 1 (PDF 316 KB)
13738_2018_1574_MOESM2_ESM.docx (23 kb)
Supplementary material 2 (DOCX 22 KB)
13738_2018_1574_MOESM3_ESM.docx (26 kb)
Supplementary material 3 (DOCX 26 KB)

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Copyright information

© Iranian Chemical Society 2019

Authors and Affiliations

  1. 1.Department of Chemical Engineering, Faculty of EngineeringUniversity of BojnordBojnordIran
  2. 2.Department of Chemical EngineeringTarbiat Modares UniversityTehranIran

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