Journal of the Iranian Chemical Society

, Volume 10, Issue 6, pp 1103–1112 | Cite as

Zinc–aluminum layered double hydroxide as a nano-sorbent for removal of Reactive Yellow 84 dye from textile wastewater effluents

  • Hossein Abdolmohammad-Zadeh
  • Ebrahim Ghorbani
  • Zeynab Talleb
Original Paper
First Online:
Received:
Accepted:

Abstract

In this research, the zinc–aluminum layered double hydroxide (Zn–Al LDH) was synthesized and structurally and morphologically characterized by X-ray diffraction, Fourier transform infrared spectroscopy, transmission electron microscopy and N2 adsorption–desorption techniques. The obtained nano-structured inorganic material was employed as an innovative nano-sorbent for separation of Reactive Yellow 84 (RY84) dye from aqueous solutions, which can be spectrophotometrically monitored at λ = 359 nm. The effect of several parameters such as type of interlayer anion in Zn–Al LDH structure, pH, sample flow rate, elution conditions, amount of nano-sorbent, sample volume and co-existing ions on the retention efficiency was investigated and optimized. The results showed that trace amounts of the RY84 could be retained using a column packed with 300 mg of the Zn–Al(NO3 −) LDH at pH 8 and stripped by 2.5 mL of 3.0 mol L−1 NaOH. Under the optimum experimental conditions, the limit of detection and the relative standard deviation were 0.04 μg mL−1 and 1.8 %, respectively. The calibration graph using the presented solid phase extraction system was linear in the range of 0.15–1.5 μg mL−1 with a correlation coefficient of 0.9982. The method was successfully applied to removal of RY84 from several textile wastewater effluents.

Keywords

Reactive Yellow 84 dye Zinc–aluminum layered double hydroxide Nano-sorbent Solid phase extraction Textile wastewater samples 
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Notes

Acknowledgments

The financial support from the Research Council of Azarbaijan Shahid Madani University (ASMU, Iran) is gratefully acknowledged.

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Copyright information

© Iranian Chemical Society 2013

Authors and Affiliations

  • Hossein Abdolmohammad-Zadeh
    • 1
  • Ebrahim Ghorbani
    • 2
  • Zeynab Talleb
    • 1
  1. 1.Department of Chemistry, Faculty of SciencesAzarbaijan Shadid Madani UniversityTabrizIran
  2. 2.Department of ChemistryPayame Nour University of TabrizTabrizIran

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