Antioxidant characteristics of extracts of Hibiscus sabdariffa calyces encapsulated with mesquite gum
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Abstract
This study compared the stability of extracts of H. sabdariffa calyces microencapsulated with different concentrations of mesquite gum during storage. Dry Roselle calyces were mixed with 50:50 (v/v) ethanol:water solution to obtain 18°Bx concentrate. This Roselle extract concentrate was mixed with purified mesquite gum (100:1–100:5 v/w). The Roselle extract concentrate-gum (RECG) was spray dried at inlet and outlet temperatures of 180 ± 2 and 104 ± 2.3 °C, respectively, at an air flow rate of 38 m3/h. Encapsulated Roselle powders (ERP) were analyzed for moisture content, total monomeric anthocyanins (differential pH), phenolic compounds (Folin and Ciocalteu method), antioxidant capacity (ABTS), and color parameters (\( L^{*} ,a^{*} \), and \( b^{*} \)) after 5 weeks and 1 year of storage. Sorption properties (isotherms) and micrographs of powders were also obtained. The average yield of RECG powders was 15.27 ± 0.81 g/100 mL. During storage, ERP showed average values of phenolic compounds, antioxidant capacity, and anthocyanins of 3.43 ± 0.25 g gallic acid equivalents/100 g, 9.34 ± 1.4 g Trolox equivalents/100 g, and 318.7 ± 20.6 mg cyanidin-O-glycoside/100 g, respectively. Color parameters remained constant along the storage time.
Keywords
Roselle powders Hibiscus sabdariffa calyces Microencapsulated Phenolic compounds Antioxidants Anthocyanins Mesquite gumNotes
Acknowledgements
This research was part of the Project Number 2006/62275-Z supported by the National Council of Science and Technology (CONACyT) in Mexico. Author Claudia Salazar-González would like to thank to CONACyT for the economic support provided for the completion of her bachelor studies. Mesquite gum was donated by Dr. J. Vernon-Carter from the Universidad Autónoma Metropolitana, Iztapalapa, Mexico City.
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