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Enhancing Mechanical Properties of Glass Ionomer Cements with Basalt Fibers

  • Xiaozhen Bao
  • Sufyan K. Garoushi
  • Fang Liu
  • Lippo L. J. Lassila
  • Pekka K. Vallittu
  • Jingwei HeEmail author
Original Paper
  • 5 Downloads

Abstract

With the aim to reinforce mechanical properties of glass ionomer cements (GICs), basalt fibers (BF, Ф13.3 μm) with 1 mm and 2 mm length were added into glass powders of commercial self-cure GIC Fuji IX with a series of mass fraction to prepare BF reinforced GICs. Fuji IX without BF was used as control. The influences of BF fibers length and mass fraction on flexural strength (FS), flexural modulus (FM), compressive strength (CS) and fracture toughness (FT) were investigated. The results showed that BF could reinforce mechanical properties of GIC significantly (p < 0.05), and the BF reinforced GIC with 7 wt.% (mass ratio in glass powders of GIC) of 2 mm fibers had the optimal mechanical properties in this research. Water sorption (WS), solubility (SL), and flexural properties after water aging of optimal BF reinforced GIC were then investigated and compared with control GIC. The FS of BF reinforced GIC decreased with the increasing of water aging time (p < 0.05), and became comparable with that of control GIC after 1 month of aging time (p > 0.05), while FMs of BF reinforced GIC and control GIC were comparable with each other (p > 0.05) and had no variation after water aging (p > 0.05). The WS of BF reinforced GIC was higher than that of control GIC (p < 0.05), but there was no significant difference in SL between these two GICs (p > 0.05). In conclusion, BF could be used to reinforce GIC, but the weak interaction between fibers and cement matrix would influence its long-time serving properties, thus further study concerned about increasing interaction between fibers and cement matrix should be taken.

Keywords

Glass ionomer cements Basalt fibers Mechanical properties Reinforcement Water aging 

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Notes

Acknowledgements

This work was funded by the National Natural Science Foundation (No.81970974) of China.

References

  1. 1.
    Fonseca RB, Branco CA, Quagliatto PS, Gonçalves LDS, Soares CJ, Carlo HL, Correr-Sobrinho L (2010) Influence of powder/liquid ratio on the radiodensity and diametral tensile strength of glass ionomer cements. J Appl Oral Sci 18(6):577–584PubMedPubMedCentralCrossRefGoogle Scholar
  2. 2.
    Garoushi S, Vallittu P, Lassila L (2017) Hollow glass fibers in reinforcing glass ionomer cements. Dent Mater 33(2):e86–e93PubMedCrossRefGoogle Scholar
  3. 3.
    Sayyedan FS, Fathi MH, Edris H, Doostmohammadi A, Mortazavi V, Hanifi A (2014) Effect of forsterite nanoparticles on mechanical properties of glass ionomer cements. Ceram Int 40(7):10743–10748CrossRefGoogle Scholar
  4. 4.
    Moshaverinia A, Ansari S, Roohpour N, Reshad M, Schricker SR, Chee WW (2011) Effects of N-vinylcaprolactam containing polyelectrolytes on hardness, fluoride release and water sorption of conventional glass ionomers. J Prosthet Dent 105(5):323–331PubMedCrossRefGoogle Scholar
  5. 5.
    Xie D, Brantley WA, Culbertson BM, Wang G (2000) Mechanical properties and microstructures of glass-ionomer cements. Dent Mater 16(2):129–138PubMedCrossRefGoogle Scholar
  6. 6.
    Munhoz T, Karpukhina N, Hill RG, Law RV (2010) Setting of commercial glass ionomer cement Fuji IX by 27Al and 19F MAS-NMR. J Dent 38(4):325–330PubMedCrossRefGoogle Scholar
  7. 7.
    Yamazaki T, Brantley W, Culbertson B, Seghi R, Schricker S (2005) The measure of wear in N-vinyl pyrrolidinone (NVP) modifed glass-ionomer cements. Polym Adv Technol 16(2–3):113–116CrossRefGoogle Scholar
  8. 8.
    Elsaka SE, Hamouda IM, Swain MV (2011) Titanium dioxide nanoparticles addition to a conventional glass-ionomer restorative: influence on physical and antibacterial properties. J Dent 39(9):589–598PubMedCrossRefGoogle Scholar
  9. 9.
    Garcia-Contreras R, Scougall-Vilchis RJ, Contreras-Bulnes R, Kanda R, Nakajima H (2014) Effects of TiO2 nano glass ionomer cements against normal and cancer oral cells. In Vivo 28(5):895–907PubMedPubMedCentralGoogle Scholar
  10. 10.
    Petri DFS, Donegá J, Benassi AM, Bocangel JAJS (2007) Preliminary study on chitosan modified glass ionomer restoratives. Dent Mater 23(8):1004–1010PubMedCrossRefGoogle Scholar
  11. 11.
    Kumar RS, Ravikumar N, Kavitha S, Mahalaxmi S, Jayasree R, Kumar TSS, Haneesh M (2017) Nanochitosan modified glass ionomer cement with enhanced mechanical properties and fluoride release. Int J Biol Macromol 104:1860–1865CrossRefGoogle Scholar
  12. 12.
    Silva RM, Pereira FV, Mota FAP, Watanabe E, Soares SMCS, Santos MH (2016) Dental glass ionomer cement reinforced by cellulose microfibers and cellulose nanocrystals. Mater Sci Eng C 58:389–395CrossRefGoogle Scholar
  13. 13.
    Alatawi RAS, Elsayed NH, Mohamed WS (2018) Influence of hydroxyapatite nanoparticles on the properties of glass ionomer cement. J Mater Res Technol.  https://doi.org/10.1016/j.jmrt.2018.01.010 CrossRefGoogle Scholar
  14. 14.
    Hammouda IM (2009) Reinforcement of conventional glass-ionomer restorative material with short glass fibers. J Mech Behav Biomed Mater 2(1):73–81PubMedCrossRefPubMedCentralGoogle Scholar
  15. 15.
    Garoushi SK, He J, Vallittu PK, Lassila LV (2018) Effect of discontinuous glass fibers on mechanical properties of glass ionomer cement. Acta Biomaterialia Odontologica Scandinavica 4(1):72–80PubMedPubMedCentralCrossRefGoogle Scholar
  16. 16.
    Deák T, Czigány T (2009) Chemical composition and mechanical properties of basalt and glass fibers: a comparison. Text Res J 79(7):645–651CrossRefGoogle Scholar
  17. 17.
    Ross A (2006) Basalt fibers: alternative to glass? Compos Technol 12(4)Google Scholar
  18. 18.
    Iorio M, Santarelli ML, González-Gaitano G, González-Benito J (2018) Surface modification and characterization of basalt fibers as potential reinforcement of concretes. Appl Surf Sci 427:1248–1256CrossRefGoogle Scholar
  19. 19.
    Manikandan V, Jappes JTW, Kumar SMS, Amuthakkannan P (2012) Investigation of the effect of surface modifications on the mechanical properties of basalt fibre reinforced polymer composites. Compos Part B 43(2):812–818CrossRefGoogle Scholar
  20. 20.
    Dhand V, Mittal G, Rhee KY, Park SJ, Hui D (2015) A short review on basalt fiber reinforced polymer composites. Compos Part B 73:166–180CrossRefGoogle Scholar
  21. 21.
    Novitskii AG (2004) High-temperature heat-insulating materials based on fibers from basalt-type rock materials. Refract Ind Ceram 45(2):144–146CrossRefGoogle Scholar
  22. 22.
    Chen X, Zhang Y, Huo H, Wu Z (2018) Study of high tensile strength of natural continuous basalt fibers. J Nat Fibers:1–9Google Scholar
  23. 23.
    Wei B, Cao H, Song S (2010) Tensile behavior contrast of basalt and glass fibers after chemical treatment. Mater Des 31(9):4244–4250CrossRefGoogle Scholar
  24. 24.
    Militký J, Kovačič V, Rubnerova J (2002) Influence of thermal treatment on tensile failure of basalt fibers. Eng Fract Mech 69(9):1025–1033CrossRefGoogle Scholar
  25. 25.
    Deák T, Czigány T, Maršálková M, Militký J (2010) Manufacturing and testing of long basalt fiber reinforced thermoplastic matrix composites. Polym Eng Sci 50(12):2448–2456CrossRefGoogle Scholar
  26. 26.
    Bashtannik PI, Kabak AI, Yakovchuk YY (2003) The effect of adhesion interaction on the mechanical properties of thermoplastic basalt plastics. Mech Compos Mater 39(1):85–88CrossRefGoogle Scholar
  27. 27.
    Botev M, Betchev H, Bikiaris D, Panayiotou C (1999) Mechanical properties and viscoelastic behavior of basalt fiber-reinforced polypropylene. J Appl Polym Sci 74(3):523–531CrossRefGoogle Scholar
  28. 28.
    Czigány T (2005) Basalt fiber reinforced hybrid polymer composites//materials science forum. Trans Tech Publ 473:59–66Google Scholar
  29. 29.
    Garoushi S, Säilynoia E, Vallittu PK, Lassila LVJ (2013) Physical properties and depth of cure of a new short fiber reinforced composite. Dent Mater:835–841PubMedCrossRefGoogle Scholar
  30. 30.
    Ghasemzadehbarvarz M, Duchesne C, Rodrigue D (2015) Mechanical, water sorption, and aging properties of polypropylene/flax/glass fiber hybrid composites. J Compos Mater 49:3781–3798CrossRefGoogle Scholar
  31. 31.
    Sharafeddin F, Tondari A, Alavi AA (2013) The effect of adding glass and polyethylene fibers on flexural strength of three types of glass-Ionomer cements. Res J Biologic Sci 8:66–70Google Scholar
  32. 32.
    Li Q, Tang C, Liu F, He J (2018) The physiochemical properties of dental resin composites reinforced with milled E-glass fibers. Silicon 10(5):1999–2007CrossRefGoogle Scholar
  33. 33.
    Xie D, Brantley WA, Culbertson BM, Wang G (2000) Mechanical properties and microstructure of glass-ionomer cements. Dent Mater 16:129–138PubMedCrossRefGoogle Scholar
  34. 34.
    Dowling AH, Fleming G, McGinley EL, Addison O (2012) Improving the standard of the standard for glass ionomer: an alternative to the compressive fracture strength test for consideration. J Dent 40:189–201PubMedCrossRefGoogle Scholar
  35. 35.
    Garoushi S, Vallittu PK, Lassila L (2011) Fracture toughness, compressive strength and load-bearing capacity of short glass fibre-reinforced composite resin. Chin J Dental Res 14:15–24Google Scholar
  36. 36.
    Dyer SR, Lassila LV, Jokinen M, Vallittu PK (2004) Effect of fibre position and orientation on fracture load of fibre-reinforced composite. Dent Mater 20:947–955PubMedCrossRefGoogle Scholar
  37. 37.
    Algera TJ, Kleverlaan CJ, Prahl-Andersen B, Feilzer AJ (2006) The influence of environmental conditions on the material properties of setting glass-ionomer cements. Dent Mater 22(9):852–856PubMedCrossRefGoogle Scholar
  38. 38.
    Culbertson BM (2001) Glass-ionomer dental restoratives. Prog Polym Sci 26(4):577–604CrossRefGoogle Scholar
  39. 39.
    Moshaverinia A, Roohpour N, Rehman IU (2009) Synthesis and characterization of a novel fast-set proline-derivative-containing glass ionomer cement with enhanced mechanical properties. Acta Biomater 5(1):498–507PubMedCrossRefPubMedCentralGoogle Scholar
  40. 40.
    Miyazaki M, Moore BK, Onose H (1996) Effect of surface coatings on flexural properties of glass ionomers. Eur J Oral Sci 104(5–6):600–604PubMedCrossRefGoogle Scholar
  41. 41.
    Miettinen VM, Vallittu PK (1997) Water sorption and solubility of glass fiber reinforced denture polymethyl methacrylate resin. J Prosthet Dent 77:531–534PubMedCrossRefGoogle Scholar
  42. 42.
    Miettinen VM, Narva K, Vallittu PK (1999) Water sorption, solubility and post-curing of glass fibre reinforced polymers. Biomaterials 20:1187–1194PubMedCrossRefGoogle Scholar
  43. 43.
    Lee SO, Rhee KY, Park SJ (2015) Influence of chemical surface treatment of basalt fibers on interlaminar shear strength and fracture toughness of epoxy-based composites. J Ind Eng Chem 32:153–156CrossRefGoogle Scholar
  44. 44.
    Kobayashi M, Kon M, Miyai K, Asaoka K (2000) Strengthening of glass-ionomer cement by compounding short fibres with CaO-P2O5-SiO2-Al2O3 glass. Biomaterials 21(20):2051–2058PubMedCrossRefGoogle Scholar
  45. 45.
    Matkó S, Anna P, Marosi G, Szep A, Keszei S, Czigany T, Pölöskei K (2003) Use of reactive surfactants in basalt fiber reinforced polypropylene composites//macromolecular symposia. Weinheim: WILEY-VCH Verlag 202(1): 255–268Google Scholar

Copyright information

© Springer Nature B.V. 2019

Authors and Affiliations

  • Xiaozhen Bao
    • 1
  • Sufyan K. Garoushi
    • 2
  • Fang Liu
    • 1
  • Lippo L. J. Lassila
    • 2
  • Pekka K. Vallittu
    • 2
    • 3
  • Jingwei He
    • 1
    • 2
    Email author
  1. 1.College of Materials Science and EngineeringSouth China University of TechnologyGuangzhouChina
  2. 2.Department of Biomaterials Science and Turku Clinical Biomaterials Center-TCBC, Institute of DentistryUniversity of TurkuTurkuFinland
  3. 3.City of Turku Welfare DivisionOral Health CareTurkuFinland

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