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, Volume 2, Issue 2, pp 79–85 | Cite as

Experimental Novel Silane System in Adhesion Promotion between Dental Resin and Pretreated Titanium. Part II: Effect of Long-Term Water Storage

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Original Paper
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Abstract

In this study we have assessed the effect of long-term water storage at 37oC on silane-aided adhesion promotion. Five experimental silane blends were evaluated as adhesion-promoters. First, five functional organosilane monomers (silicon esters), 3-acryloxypropyltrimethoxysilane, 3-methacryloxypropyltrimethoxysilane, 3-glycidoxypropyltrimethoxysilane, tetrakis-(2-methacryloxyethoxy)silane and bis-[3-(triethoxysilyl)propyl]tetrasulfide, were diluted to 1% (v/v) in 95% ethanol and blended with a non-functional cross-linking silane, bis-1,2-(triethoxysilyl)ethane (1%). A commercially available pre-activated silane product was used as the control. After activation by hydrolysis, each primer blend was applied to silica-coated Ti coupons. Stubs of experimental bis-phenol-A-diglycidyldimethacrylate (bis-GMA)-based resin were bonded by photo-polymerization onto the pretreated Ti coupons. Half of the specimens were stored in deionized water for 6 months and half for 12 months. The primer containing 3-acryloxypropyltrimethoxysilane and bis-1,2-(triethoxysilyl)ethane produced significantly higher shear bond strengths than the control silane and other experimental silane primers after both periods of storage.

Keywords

Silica-coating Silica Silane coupling agent Silane monomer Titanium Water-storage 
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References

  1. 1.
    Meiners H, Herrmann R, Spitzbarth S (1990) Dent-Labor 38:185Google Scholar
  2. 2.
    Matinlinna J, Lassila LVJ, Özcan M, Yli-Urpo A, Vallittu PK (2004) Int J Prosthodont 17:155Google Scholar
  3. 3.
    Rosen MR (1978) J Coat Technol 50:70Google Scholar
  4. 4.
    Plueddemann EP (1982) Silane coupling agents. Plenum, New YorkGoogle Scholar
  5. 5.
    Sundararajan PG, van Ooij WJ (2000) Surf Eng 16:315CrossRefGoogle Scholar
  6. 6.
    van Ooij WJ, Zhu DQ, Prasad G, Jayaseelan S, Fu Y, Teredesai N (2000) Surf Eng 16:386CrossRefGoogle Scholar
  7. 7.
    Klempner D, Sperling LH, Utracki LA (1994) Interpenetrating polymer network. Advances in chemical sciences. Am Chem Soc, Washington, Vol. 239Google Scholar
  8. 8.
    Matinlinna JP, Lassila LVJ, Vallittu PK (2007) Dent Mater 23:1173CrossRefGoogle Scholar
  9. 9.
    Matinlinna JP, Lassila LVJ, Vallittu PK (2007) Acta Odontol Scand 65:44CrossRefGoogle Scholar
  10. 10.
    Bowen RL, Marjenhoff WA (1992) Adv Dent Res 6:44Google Scholar
  11. 11.
    Kern M, Thompson VP (1994) J Dent 22:300CrossRefGoogle Scholar
  12. 12.
    Kern M, Thompson VP (1995) J Prosthodont 4:16CrossRefGoogle Scholar
  13. 13.
    Matinlinna JP, Lassila LVJ, Kangasniemi I, Yli-Urpo A, Vallittu PK (2005) Dent Mater 21:287CrossRefGoogle Scholar
  14. 14.
    Matinlinna JP, Lassila LV, Vallittu PK (2010) Experimental novel silane system in adhesion promotion between dental resin and pretreated titanium. Silicon 1:249–254CrossRefGoogle Scholar
  15. 15.
    Puska M, Lassila L, Seppälä J, Vallittu P, Matinlinna J (2009) J Adhes Sci Technol 23:991CrossRefGoogle Scholar
  16. 16.
    International Organization for Standardization (ISO) (1996) Dentistry-polymer-based crown and bridge materials, Amendment 1996; ISO 10477Google Scholar
  17. 17.
    Darvell BW (1978) J Oral Rehabil 5:41CrossRefGoogle Scholar
  18. 18.
    Matinlinna JP, Lassila LVJ, Vallittu PK (2006) J Dent 34:740CrossRefGoogle Scholar
  19. 19.
    Matinlinna JP, Dahl JE, Lassila LVJ, Vallittu PK (2007) In: Mittal KL (ed) Silanes and other coupling agents, vol. 4. pp 83–97Google Scholar
  20. 20.
    Matinlinna JP, Lassila LVJ, Kangasniemi I, Vallittu PK (2005) J Dent Res 84:360CrossRefGoogle Scholar
  21. 21.
    Plueddemann EP (1968) J Paint Technol 40:1Google Scholar
  22. 22.
    Bikerman JJ (1967) Ind Eng Chem 59:41CrossRefGoogle Scholar
  23. 23.
    Plueddemann EP (1962) Mod Plast 39:135Google Scholar
  24. 24.
    Plueddemann EP (1970) Mod Plast 47:92Google Scholar
  25. 25.
    van Noort R (2007) Introduction to dental materials, 3rd edn. Mosby Elsevier, EdinburghGoogle Scholar
  26. 26.
    Matinlinna JP, Mittal KL (eds) (2009) Adhesion aspects in dentistry. VSP/Brill, LeidenGoogle Scholar
  27. 27.
    Söderholm K-J (2009) J Adhes Sci Technol 23:973CrossRefGoogle Scholar
  28. 28.
    Darvell BW (2009) J Adhes Sci Technol 23:935CrossRefGoogle Scholar

Copyright information

© The Author(s) 2010

Authors and Affiliations

  1. 1.Dental Materials Science, Faculty of Dentistry, The University of Hong KongThe Prince Philip Dental HospitalHong KongPeople’s Republic of China
  2. 2.Department of Biomaterials Science, Institute of DentistryThe University of TurkuTurkuFinland

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