Metallurgical and Materials Transactions A

, Volume 50, Issue 12, pp 5574–5580 | Cite as

Oxidation-Related Microstructural Changes at a Crack Tip in Waspaloy After Elevated-Temperature Dwell-Fatigue Testing

  • G. B. ViswanathanEmail author
  • David E. Mills
  • Michael J. Mills


Using advanced aberration-corrected scanning transmission electron microscopy coupled with high-resolution energy-dispersive spectroscopy techniques, transitions to microstructure and composition occurring at a grain boundary (GB) crack-tip in Waspaloy after dwell-fatigue at 704 °C are characterized at the nano to atomic scale. The simple microstructure of this γ/γ′ superalloy, which enables elucidation of oxygen effect ahead of the oxide intrusion—dissolution of the precipitates fostering selective segregation of Al to the GB to form oxides—has been experimentally observed.


The authors would like to thank Rolls-Royce Corporation for their material and financial supports for this research.


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Copyright information

© The Minerals, Metals & Materials Society and ASM International 2019

Authors and Affiliations

  • G. B. Viswanathan
    • 1
    Email author
  • David E. Mills
    • 2
  • Michael J. Mills
    • 1
  1. 1.Department of Materials Science and EngineeringThe Ohio State UniversityColumbusUSA
  2. 2.Rolls-Royce CorporationIndianapolisUSA

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